Table 1.
Factor | Ultra-Turrax Pretreatment |
Ultrasound-Assisted Pretreatment |
||||
---|---|---|---|---|---|---|
−1 | 0 | +1 | −1 | 0 | +1 | |
Stirring rate (rpm) (X1) | 10,000 | 20,000 | 30,000 | |||
Sample mass (g) (X2) | 0.3 | 0.6 | 0.9 | |||
Solvent concentration (%v/v) (X3) | 40 | 60 | 80 | |||
Time (sec) (X4) | 30 | 60 | 90 | |||
Sample mass (g) (X1) | 0.3 | 0.6 | 0.9 | |||
Solvent concentration (%v/v) (X2) | 40 | 60 | 80 | |||
Time (sec) (X3) | 10 | 20 | 30 | |||
Temperature (°C) (X4) | 30 | 50 | 70 |