Table 1.
Material (Manufacturer) Code | Composition | Lot number | Fillers % | Manufacturer recommendation |
---|---|---|---|---|
Clearfil Tri-S Bond Plus adhesive One-step self-etch (Kuraray Noritake Dental, Japan) TP |
Adhesive: MDP, Bis-GMA, HEMA, hydrophilic aliphatic dimethacrylate, hydrophobic aliphatic methacrylate, colloidal silica, sodium fluoride, dl-camphorquinone, accelerators, initiators, ethanol, water, others (pH = 2.3). | 00007A | — |
Adhesive
(i) Apply bond for 10 s (ii) Dry with mild pressure air flow for 5 s (iii) Light cure for 10 s |
Estelite Sigma Quick Universal composite (Tokuyama Dental, Japan) EQ |
Composite: Bis-GMA, TEGDMA, silica–zirconia fillers, silica–titania fillers, photoinitiators. | J018 | 82% (wt.) 71% (vol) |
Composite
(i) Light cure the composite for 10 s, keeping the curing light tip within a distance of 2 mm from the surface |
Silorane system adhesive Two-step self-etch (3M ESPE, USA) SA |
Primer: phosphorylated methacrylates, Vitrebond copolymer, Bis-GMA, HEMA, water, ethanol, silane-treated silica filler, initiators, stabilizers (pH: 2.7). | N289224 | — |
Primer
(i) Apply primer for 15 s (ii) Gentle air dry (iii) Light cure for 10 s |
Bond: hydrophobic dimethacrylate, phosphorylated methacrylates, TEGDMA, silane-treated silica filler, initiators, stabilizers. | N209848 | — |
Bond
(i) Apply bond (ii) Gentle air dry (iii) Light cure for 10 s |
|
Filtek Silorane Low shrinkage posterior composite (3M ESPE, USA) FS |
Composite: silorane resin, CQ, iodonium salt, electron donor, quartz filler, yttrium fluoride, stabilizers, pigments. | N204592 | 76% (wt.) 55% (vol) |
Composite
(i) Light cure the composite for 20 s, keeping the curing light tip within a distance of 2 mm from the surface |
HEMA: 2-hydroxyethyl methacrylate; Bis-GMA: bisphenol-A-diglycidyl methacrylate; TEGDMA: triethyleneglycoldimethacrylate; MDP: 10-methacryloyloxydecyl dihydrogen phosphate; CQ: camphorquinone; wt: weight; vol: volume.