Table 2. Details of Rietveld Refinement of As-Made ITQ-56.
| parameters | |
|---|---|
| crystal system | orthorhombic |
| space group | Immm (71) |
| a (Å) | 13.5076 |
| b (Å) | 26.5882 |
| c (Å) | 55.4883 |
| λ (Å) | 0.39984 |
| temperature (°C) | 20 |
| 2θ range (deg) | 0.75–20.0 |
| resolution (Å) | 1.15 |
| no. of restraints | 78 for T–O, 120 for O–T–O, 46 T–O–T |
| no. of reflections | 3807 |
| Rwp | 0.149 |
| Rexp | 0.057 |
| GoF | 2.64 |