Table 2.
Completion of automated SPPS
| No. | Action | Reagent | Solvent | Vol. [μL] | Time [min] | Repeats |
|---|---|---|---|---|---|---|
| 1 | Deprotection | 20% (v/v) Pip | DMF | 4 | 10 | 2× |
| 2 | Wash | DMF | 400 | - | 7× | |
| 3 | Wash | EtOH | 400 | - | 2× | |
| 4 | Wash | EtOH | 600 | - | 2× | |
| 5 | Wash | EtOH | 400 | - | 3× | |
| 6 | Extract | - | - | 10 | - |
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