Table 1.
Data collection and refinement statistics
| DNAJC9 HBD-H3.3-H4-MCM2 HBD (7CJ0) | DNAJC9 αB-H3.3-H4-MCM2 HBD (7CIZ) | |
|---|---|---|
| Data collection | ||
| Space group | P3121 | C2221 |
| Cell dimensions | ||
| a, b, c (Å) | 47.5, 47.5, 616.3 | 47.6, 176.8, 202.9 |
| α, β, γ (°) | 90, 90, 120 | 90, 90, 90 |
| Resolution (Å) | 41.08–2.24 (2.30–2.24)a | 40–1.80 (1.83–1.80)a |
| No. reflections (total/unique) | 716,208/41,413 | 781,980/78,310 |
| Rpim (%) | 2.2 (51.9) | 2.4 (40.0) |
| I/σI | 17.7 (1.9) | 31.3 (2.2) |
| Completeness (%) | 99.9 (99.1) | 97.7 (91.2) |
| Redundancy | 17.3 (16.8) | 10.0 (9.5) |
| Refinement | ||
| Resolution (Å) | 41.08–2.50 | 36.88–1.80 |
| No. reflections (unique) | 29,934 | 77,571 |
| Rwork/Rfree (%) | 25.8/29.5b | 17.1/21.4 |
| No. atoms | ||
| Protein | 4,621 | 5,956 |
| GOL | 6 | |
| SO4 | 10 | |
| Water | 69 | 741 |
| B-factors | ||
| Protein | 79.4 | 24.0 |
| GOL | 82.1 | |
| SO4 | 62.7 | |
| Water | 69.0 | 38.9 |
| RMSDs | ||
| Bond lengths (Å) | 0.002 | 0.006 |
| Bond angles (°) | 0.45 | 0.79 |