Table 2.
Data collection and refinement statistics.
| Data processing | No. of indexed images | ||
|---|---|---|---|
| 1000 | 2000 | 3000 | |
| Resolution (Å) | 80.0–1.65 (1.71–1.65) | ||
| Unique reflections | 14,827 (1413) | 15,355 (1490) | 15,398 (1499) |
| Completeness (%) | 96.29 (94.26) | 99.72 (99.40) | 99.96 (99.80) |
| Multiplicity | 8.7 (5.9) | 17.8 (12.1) | 28.9 (19.7) |
| SNR | 3.00 (1.13) | 3.43 (1.28) | 4.25 (1.61) |
| CC | 0.8116 (0.3654) | 0.8792 (0.4508) | 0.9277 (0.5570) |
| CC* | 0.9465 (0.7316) | 0.9673 (0.7883) | 0.9810 (0.8458) |
| Rsplit (%) | 37.53 (110.47) | 28.69 (81.67) | 21.50 (67.10) |
| Molecular replacement | |||
| Top LLG | 3361.874 | 5053.713 | 6122.978 |
| Top TFZ | 53.6 | 60.1 | 62.4 |
| Refinement | |||
| Resolution (Å) | 56.18–1.65 (1.73–1.665) | ||
| Rwork | 0.2993 (0.4063) | 0.2500 (0.3357) | 0.2162 (0.3104) |
| Rfree | 0.3563 (0.4110) | 0.2935 (0.3977) | 0.2599 (0.3463) |