TABLE 2.
13C NMR data of compounds 1–6 in CDCl3 at 150 MHz.
No. | 1 | 2 | 3 | 4 | 5 | 6 |
1 | 138.5, C | 138.8, C | 138.4, C | 138.0, C | 45.0, CH | 140.8, C |
2 | 125.0, C | 125.6, C | 125.8, C | 125.2, C | 162.9, C | 132.6, C |
3 | 43.56, CH | 44.5, CH | 44.6, CH | 43.6, CH | 128.8, C | 44.7, CH |
4 | 26.5, CH2 | 22.7, CH2 | 22.6, CH2 | 26.5, CH2 | 20.1, CH2 | 22.2, CH2 |
5 | 33.1, CH2 | 36.9, CH2 | 36.9, CH2 | 33.2, CH2 | 33.5, CH2 | 36.9, CH2 |
6 | 32.7, CH | 31.5, CH | 31.5, CH | 32.6, CH | 32.7, CH | 30.7, CH |
7 | 43.59, CH | 48.4, CH | 47.7, CH | 43.2, CH | 41.5, CH | 47.5, CH |
8 | 40.8, CH2 | 40.1, CH2 | 39.7, CH2 | 40.6, CH2 | 42.3, CH2 | 41.1, CH2 |
9 | 42.6, C | 43.8, C | 43.9, C | 42.8, C | 39.0, C | 42.6, C |
10 | 41.2, CH2 | 41.5, CH2 | 41.6, CH2 | 41.1, CH2 | 83.6, CH | 80.1, CH |
11 | 69.20, CH2 | 69.6, CH2 | 69.6, CH2 | 69.2, CH2 | 71.1, CH2 | 68.9, CH2 |
12 | 177.8, C | 179.3, C | 179.3, C | 177.8, C | 175.3, C | 178.6, C |
13 | 17.5, CH3 | 12.0, CH3 | 12.1, CH3 | 17.7, CH3 | 12.1, CH3 | 12.9, CH3 |
14 | 24.3, CH3 | 23.6, CH3 | 22.7, CH3 | 23.2, CH3 | 23.9, CH3 | 22.1, CH3 |
15 | 69.18, CH2 | 68.9, CH2 | 71.2, CH2 | 71.5, CH2 | 29.1, CH3 | 25.7, CH3 |