Table 2.
1H NMR (400 MHz) and 13C NMR (100 MHz) data for fusarins I (3) and J (4) in CDCl3.
| No. | 3 | 4 | ||
|---|---|---|---|---|
| δC Type | δH (J in Hz) | δC Type | δH (J in Hz) | |
| 1 | 16.0 CH3 | 1.74 (d 7.3) | 14.6 CH3 | 1.92 (d 7.2) |
| 2 | 140.5 CH | 6.98 (q 7.1) | 141.1 CH | 7.05 (q 7.2) |
| 3 | 130.5 | 131.8 | ||
| 4 | 127.1 CH | 6.18 (s) | 71.8 CH | 5.06 (d 10.5) |
| 5 | 138.1 | 144.2 | ||
| 6 | 140.6 CH | 6.58 (m) | 123.7 CH | 6.28 (d 11.4) |
| 7 | 128.6 CH | 6.43 (dd 15.2, 10.3) | 137.5 CH | 6.86 (dd 14.7, 11.4) |
| 8 | 140.6 CH | 6.66(dd 14.6, 10.4) | 130.6 CH | 6.34 (dd 14.7, 11.2) |
| 9 | 127.9 CH | 6.55 (d 14.7) | 143.9 CH | 7.20 (dd 15.4, 11.1) |
| 10 | 140.9 CH | 7.37 (d 11.3) | 129.8 CH | 6.13 (d 15.4) |
| 11 | 126.0 | 198.6 | ||
| 12 | 173.6 | 27.5 CH3 | 2.27 (s) | |
| 13 | 167.7 | 167.8 | ||
| 14 | 52.1 OCH3 | 3.74 (s) | 52.1 OCH3 | 3.74 (s) |
| 15 | 14.4 CH3 | 1.70 (s) | 14.5 CH3 | 1.80 (d 1.3) |
| 16 | 12.5 CH3 | 1.98 (s) | ||