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. 2021 Jun 1;11(6):1469. doi: 10.3390/nano11061469

Table 2.

Overview of reported length reduction of CNT due to sonication, indicating the solvent system, the type of CNT, sonication power, and energy applied, as well as determined damage, together with the respective citation.

Dispersion Medium Nanofiller Type Input Power Sonication Time/Energy Input Analyzing Tool Length Reduction Measured Dimension Citation
Distilled water + polyacrylate-based dispersing agent MWCNT 150 W 25 J/mL–400 J/mL SEM 265 nm (75 J/mL)–216 nm (400 J/mL); histogram peak Length [35]
Milli-Q water Carboxylated MWCNT 100 W 7 h SEM 902 nm (0 min)–152 nm Length [87]
Distilled water MWCNT 260 W, ultrasonic bath 15–120 min DLS 400 nm (0 min)–50 nm (90 min) Length calculated from Dh [70]
D2O + sodium cholate SWCNT 20 W 5–120 min AFM 800 nm (0 min)–165 nm (120 min) Length [36]
Sodium deoxychlorate SWCNT 120 W, sonication tip 10–120 min AFM 1.3 µm (30 min)–0.7 µm (120 min) histogram peak Length [69]
Organic solvent + pyrene-siloxane surfactant MWCNT >60 W/cm2 3–10 h SEM 5–15 µm (0 min)–2–6 µm (3 h) Length [65]
Sodium dodecyl sulfate + Milli-Q water SWCNT (bundles) 20 and 40 W 15–120 min DDLS Length: 2.286–1.146 µm; diameter: 40.6–12.1 nm (20 W, 30–120 min); 1.156–0.822 µm; diameter: 37.9–2.9 nm (40 W, 15–120 min); Length and diameter [78]
Water MWCNT and N-doped MWCNT 1.2 kJ, 2.1 kJ, 6 kJ, 10 kJ, 17 kJ 30–300 s SEM 17.1± 11.9 µm undoped–13.6 ± 9.9 µm N-doped (30 s, 1.2 kJ); 9.5 ± 5.1 µm undoped–10.1 ±6.0 µm N-doped (300 s, 10 kJ) Contour length [67]