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. 2021 Jun 1;11(6):1469. doi: 10.3390/nano11061469

Table 4.

Overview of the literature with respect to monitoring the dispersion state of CNT, including information on the media into which CNT were dispersed, the CNT type, sonication power, energy input or sonication time, and characterization method applied, with a short summary of the results and the according citation for further reading.

Dispersion Medium Nanofiller Type Input Power Sonication Time/Energy Input Analyzing Tool Results Citation
Various surfactants (SDS, CTAB, polyxyethylene stearyl ether) and deionized water MWCNT (neat and different functionalized types) 140 W 100 min UV–vis General finding for different surfactants and MWCNT: at short sonication time, absorbance increases rapidly, at higher times, absorbance levels off [75]
NaDOC (30% cmc and 300% cmc) in Milli-Q water SWCNT 100 and 200 W 0–60 min UV–vis 100 W: ~0.775 (15 min)–0.88 (60 min) (30% cmc) ~0.825 (15 min)~1.25 (60 min) (300% cmc)
200 W: ~0.85 (15 min)–1.0 (60 min) (30% cmc) ~1.1 (15 min) ~1.95 (60 min) (300% cmc)
[38]
17 different surfactants SWCNT 140 W 0–120 min UV–vis Resonance ratio increases: 0.04 (0 min)–0.08 (120 min) (surfactant: NaDDBS) [86]
Distilled water + polyacrylate-based dispersing agent MWCNT 150 W 25 J/mL–400 J/mL UV–vis Increase in absorbance: 0.4 (25 J/mL)–0.8 (400 J/mL) [35]
Acetone MWCNT /(ultrasonic bath) 2–42 h Rheology Increasing viscosity values with increasing sonication time [83]
Ethanol MWCNT / 2 h Rheology Shear thinning—viscosity values: ~106–~102 Pa.s (functionalized MWCNT); ~103–~101 Pa.s (neat MWCNT) [80]
DCM MWCNT 60–70 W 0–90 min UV–vis + rheology UV–vis: Increase of absorbance until 30 min sonication, afterwards decrease
Rheology: After 30 min, network formation, afterwards, negatively affected
[61]