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. 2021 Jun 10;9(6):136. doi: 10.3390/toxics9060136

Table 3.

LOD and LOQ of the 1H NMR method for the screening of cannabinoids in CBD oils.

Analyte Signal δ [ppm] LOD [mg/kg Sample] LOQ [mg/kg Sample]
CBD H-1 3.88 346 1092
H-9 cis 4.52 134 445
H-9 trans 4.63 307 979
9-THC H-3′ 6.15 608 1858
8-THC H-3′ 6.12 250 816
CBN H-2 7.05 517 1604
H-5 7.13 623 1897
H-4 8.21 504 1568