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. 2021 Jun 1;62:100089. doi: 10.1016/j.jlr.2021.100089

Table 2.

Test compounds not previously associated with phospholipidosis

Generic Name UPAC Designation CAS Number Indication ClogP pKa (basic) Ploemen Value Pred Ploemen Pred Mod
Ploemen
LPLA2 IC50 (μM)
Amisulpride 4-amino-N-[(1-ethyl-2-pyrrolidinyl)methyl]-5-(ethylsulfonyl)-2-methoxybenzamide 71675-85-9 antipsychotic 1.5 7.05 52 - - 1915
Allopurinol 3-(4H-1,2,4-triazol-4-yl)-1H-pyrazole-4-carboxamide 315-30-0 xanthine oxidase inhibitor -0.55 2.57 6.9 - - ND
Atovaquone 2-hydroxy-3-[(1r,4r)-4-(4-chlorophenyl) cyclohexyl] -1,4-dihydronaphthalene-1,4-dione 95233-18-4 anti-pneumocystis, anti-malarial 1.59 8.16 69.1 - - ND
Atropine (1R,3R,5S)-8-methyl-8-azabicyclo[3.2.1]octan-3-yl 3-hydroxy-2-phenylpropanoate 51-55-8 antimuscarinic 1.83 9.39 91.5 - - 1874
Azaperone 1-(4-fluorophenyl)-4-[4-(pyridin-2-yl)piperazin-1-yl] butan-1-one 1649-18-9 tranquilizer 2.73 7.16 58.7 - + ND
Benztropine (1R,3R,5S)-3-(diphenylmethoxy)-8-methyl-8-azabicyclo[3.2.1]octane 86-13-5 antitremor 4.27 9.54 109 + + 58.97
18 Beta-glycyrrhetinic acid 3β-hydroxy-11-oxo-18β,20β-olean-12-en-29-oic acid 471-53-4 anti-inflammatory, antioxidant 3.7 16 270 + + 2432
Butenafine [(4-tert-butylphenyl)methyl](methyl)(naphthalen-1-ylmethyl)amine 101828-21-1 antifungal 5.85 9.23 119 + + 41.2
Carbamazepine 2-azatricyclo[9.4.0.03,8]pentadeca-1(15),3,5,7,9,11,13-heptaene-2-carboxamide 298-46-4 anticonvulsant 2.77 -3.8 7.7 - - 105.6
Clomifene 2-[4-(2-chloro-1,2-diphenylethenyl) phenoxy]ethyl} diethylamine 911-45-5 estrogen agonist 7.2 9.31 139 + + 12.86
Clonidine N-(2,6-dichlorophenyl)-4,5-dihydro-1H-imidazole-2-amine 4205-90-7 antihypertensive 1.59 8.16 69.1 - - ND
Cloricromen 8-chloro-3-(2-diethylaminoethyl)-7-ethoxycarbonylmethoxy-4-methylcoumarin hydrochloride 74697-28-2 platelet aggregation inhibitor 3.97 9.1 98.6 - + 285
Conessin (3β)-N,N-dimethyl-con-5-enin-3-amine 546-06-5 antihistamine 4.9 5 49 - - 31.28
Desloratadine 13-chloro-2-(piperidin-4-ylidene)-4-azatricyclo [9.4.0.03,8] pentadeca-1(11),3(8),4,6,12,14-hexaene 100643-71-8 antihistamine 3.48 9.73 107 + + 8.36
D-(+)-glucose (2R,3S,4R,5R)-2,3,4,5,6-pentahydroxyhexanal 50-99-7 monosaccharide -2.4 -3 14.8 - - ND
Diclofenac (2-[(2,6-dichlorophenyl)amino] benzene acetic acid sodium salt-15307-79-6) 15307-79-6 nonsteroidal anti inflammatory 4.51 -2.1 20.3 - - 7.2
5,7 Dichloro-8-hydroxy-2-methyl quinolone 5,7-Dichloro-2-methyl-8-quinolinol 72-80-0 antioxidant 3.61 4 29 - - 1179
Dilazep 3-{4-[3-(3,4,5-trimethoxybenzoyloxy)propyl]-1,4-diazepan-1-yl} propyl 3,4,5-trimethoxybenzoate 35898-87-4 adenosine uptake inhibitor 3.21 9.54 101 + + 59.76
1,7-Dimethylxanthine 1,7-Dimethyl-1H-purine-2,6-dione 611-59-6 stimulant -0.8 13.5 183 - - ND
Disopyramide 4-[bis(propan-2-yl)amino]-2-phenyl-2-(pyridin-2-yl) butanamide 3737-09-5 antiarrhythmic 2.58 10.31 115 + + ND
Fenspiride 8-(2-phenylethyl)-1-oxa-3,8-diazaspiro[4.5]decan-2-one 5053-08-7 anti-inflammatory 1.81 9.37 91.1 - - ND
Fosinopril (2S,4S)-4-cyclohexyl-1-{2-[(R)-[(1S)-2-methyl-1-(propanoyloxy)propoxy](4-phenylbutyl) phosphoryl] acetyl} pyrrolidine-2-carboxylic acid 98048-97-6 Angiotensin-converting enzyme inhibitor 5.62 -4.4 31.6 - 0.181
Fosinoprilat (2S,4S)-4-cyclohexyl-1-{2-[hydroxy(4-phenylbutyl)phosphoryl]acetyl}pyrrolidine-2-carboxylic acid 95399-71-6 active fosinopril metabolite 3.7 -4.7 35.8 - - 5.764
Fulvestrant (1S,3aS,3bR,4R,9bS,11aS)-11a-methyl-4-[9-(4,4,5,5,5-pentafluoropentanesulfinyl)nonyl]-1H,2H,3H,3aH,3bH,4H,5H,9bH,10H,11H,11aH-cyclopenta[a]phenanthrene-1,7-diol 129453-61-8 chemotherapeutic 6.54 -0.88 42.8 - - 61.85
Fusidic acid (3α,4α,5α,8α,9β,11α,13α,14, 16β,17Z)-16-acetoxy-3,11-dihydroxy-4,8,14-trimethyl-18-norcholesta-17,24-dien-21-oic acid 6990-06-3 antibiotic 4.97 -0.2 24.7 - - 231
Gabapentin 2-[1-(amino methyl) cyclohexyl]acetic acid 60142-96-3 antiepileptic -1.9 9.91 102 - - 37.37
Harmine 7-methoxy-1-methyl-9H-pyrido[3,4-b]indole 442-51-3 central nervous system stimulant. 2.61 6.46 48.5 - - 633
Hydralazine 1-hydrazinylphthalazine 86-54-4 antihypertensive 1 6.4 41 - - 100
Hydrocortisone (11β)-11,17,21-trihydroxypregn-4-ene-3,20-dione 50-23-7 glucocorticoid 1.61 -2.8 10.4 - - 402
6-Hydroxy-dopamine 2,4,5-rihydroxyphenethylamine hydrochloride 28094-15-7 neurotoxin 0.26 9.85 97.1 - - 88.02
3-Hydroxy-tyramine hydrochloride 2-(3,4-dihydroxyphenyl)ethylamine hydrochloride, 3,4-dihydroxyphenethylamine hydrochloride 62-31-7 catecholamine neurotransmitter -0.91 9.27 86.9 - - 56.08
Imiquimod 1-(2-methylpropyl)-1H-imidazo[4,5-c]quinolin-4-amine 99011-02-6 topical immunomodulatory 2.83 5.01 33.1 - + 160
Isoxsuprine 4-[(1S,2R)-1-hydroxy-2-{[(2R)-1-phenoxypropan-2-yl]amino}propyl]phenol 395-28-8 vasodilator 2.06 9 85.2 - + ND
Lidocaine 2-diethylamino-N-(2,6-dimethylphenyl)acetamide 137-58-6 antiarrhythmic 1.8 7.75 63.3 - - ND
L-leucine (2S)-2-amino-4-methylpentanoic acid 61-90-5 amino acid -1.52 9.52 92.9 - - ND
Mebhydrolin 5-benzyl-2-methyl-1H,2H,3H,4H,5H-pyrido[4,3-b]indole 524-81-2 antihistamine 3.5 6.7 57.1 - + 146
Meclofenamic acid 2-[(2,6-dichloro-3-methylphenyl)amino]benzoic acid 644-62-2 nonsteroidal 5.11 -3.6 39.1 - - ND
Melatonin N-acetyl-5-methoxytryptamine 73-31-4 antigonadotrope 1.42 -1.6 4.6 - - 38.03
Mibefradil (1S,2S)-2-(2-{[3-(1H-1,3-benzodiazol-2-yl)propyl] (methyl)amino}ethyl)-6-fluoro-1-(propan-2-yl)-1,2,3,4-tetrahydronaphthalen-2-yl 2-methoxyacetate 116644-53-2 calcium channel blocker 5.34 9.82 124 + + 12.92
Naproxen (2S)-2-(6-methoxynaphthalen-2-yl) propanoic acid 22204-53-1 nonsteroidal 3.18 -4.8 33.2 - - 1102
Orphenadrine dimethyl({2-[(2-methylphenyl) (phenyl) methoxy] ethyl}) amine 83-98-7 muscle relaxant 3.77 8.87 92.9 + + 259.3
Phenytoin 5,5-diphenyl-2,4-imidazolidinedione, 5,5-Diphenylhydantoin sodium salt 630-93-3 anticonvulsant 2.47 -9 6.1 - - 60.05
Pipamperone 1′-[4-(4-fluorophenyl)-4-oxobutyl]-[1,4′-bipiperidine]-4′-carboxamide 1893-33-0 antipsychotic 2.32 8.96 85.7 - + 250
PP 06424439 (3R)-1-[2-[1-(4-chloro-1H-pyrazol-1-yl)cyclopropyl]-3H-imidazo[4,5-b]pyridin-5-yl]-3-piperidinyl]-1-pyrrolidinyl-methanone 1469284-79-4 triglyceride and cholesterol lowering 2.7 4.1 24.1 - - 8217
Prochlorperazine 2-chloro-10-[3-(4-methylpiperazin-1-yl)propyl]-10H-phenothiazine 58-38-8 antipsychotic 4.88 8.39 94.2 + + 42.41
Procyclidine 1-cyclohexyl-1-phenyl-3-(pyrrolidin-1-yl)propan-1-ol 77-37-2 anticholinergic 4.7 13.84 214 + + 1470
Ritanserin 6-(2-{4-[bis(4-fluorophenyl)methylidene]piperidin-1-yl}ethyl)-7-methyl-5H-[1,3]thiazolo[3,2-a]pyrimidin-5-one 87051-43-2 serotonin receptor agonist 5.02 8 89.2 - + 13.39
Rolipram 4-[3-(cyclopentyloxy)-4-methoxyphenyl]pyrrolidin-2-one 61413-54-5 antidepressant 2.15 -1.9 9.9 - - 300
SB222200 (S)-3-methyl-2-phenyl-N-(1-phenylpropyl)-4-quinolinecarboxamide-174635-69-9 174635-69-9 antihistamine 2.17 9.57 98.2 + + 14.94
S-methyl-isothiourea methyl carbamimidothioate 867-44-7 iNOS inhibitor 1.47 9.83 98.8 - - ND
Suloctidil (1R,2S)-2-(octylamino)-1-[4-(propan-2-ylsulfanyl)phenyl]propan-1-ol 54767-75-8 vasodilator 5.54 9.76 126 + + 6.82
Trifluoperazine 10-[3-(4-methylpiperazin-1-yl)propyl]-2-(trifluoromethyl) -10H-phenothiazine 117-89-5 antipsychotic, antiemetic 4.87 8.39 94.1 + + 6.87
Uridine 1-[(2R,3R,4S,5R)-3,4-dihydroxy-5-(hydroxymethyl) oxolan-2-yl]-1,2,3,4-tetrahydropyrimidine-2,4-dione 58-96-8 pyrimidine analog -1.98 -3 3.9 - - ND
Xylometazoline 2-[(4-tert-butyl-2,6-dimethylphenyl)methyl]-4,5-dihydro-1H-imidazole 526-36-3 decongestant 3.2 10.29 129 + + 44.32

The generic name, International Union of Pure and Applied Chemistry (IUPAC) designation, chemical abstracts registry (CAS) number, and clinical indication are provided. Chemical properties, including ClogP and pKa (basic) were obtained from the Pubchem and chEMBL database of bioactive molecules and used to calculate the Ploemen value for each compound. By convention, negative pKa values were assigned a value of 0 for calculation of the Ploemen number and would be predicted negative based on pKa values of less than 8 or 6 for the Ploemen and modified Ploemen models respectively. LPLA2 IC50 denotes the concentration at which 50% of the LPLA2 dependent 1-O-acyl N-acetylsphingosine synthase activity is observed.