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Refinement and geometric statistics.
| Resolution | 30.0–3.15 Å |
|---|---|
| Unique reflectionsa | 5771 |
| Free R set | 5.0% |
| Working reflections | 5482 |
| Rworking | 0.205 (0.231) |
| Rfree | 0.274 (0.322) |
| r.m.s.d bond lengths | 0.009 Å |
| r.m.s.d bond angles | 1.8° |
| r.m.s.d chiral vol. | 0.084 Å3 |
| Ramachandran outliers | 10, 5/molecule |
| Rotamer outliers | none |
| Water molecules | 28 |
| ligands | β octylglucoside (2) |
Data was cutoff at 3.15 Å resolution.
