TABLE 5.
The results of accuracy and precision.
Component | Concentration (ng/ml) | Intra-day precision | Inter-day precision | Accuracy | ||||
---|---|---|---|---|---|---|---|---|
Mean (ng/ml) | RSD (%) | Mean (ng/ml) | RSD (%) | Mean (ng/ml) | RE (%) | RSD (%) | ||
TSG | 14,825.00 | 14,876.26 | 4.1 | 15,023.17 | 4.2 | 15,981.35 | 7.8 | 2.3 |
741.25 | 740.84 | 6.6 | 747.81 | 6.9 | 730.87 | -1.4 | 4.1 | |
14.83 | 13.69 | 6.2 | 12.23 | 3.1 | 17.23 | 16.2 | 3.2 | |
Emodin | 38,375.00 | 38,406.12 | 6.9 | 37,697.78 | 6.3 | 19,590.44 | 2.1 | 5.9 |
767.50 | 773.6 | 3.5 | 783.09 | 1.1 | 745.24 | −2.9 | 7.7 | |
15.28 | 14.02 | 6.8 | 13.94 | 7.9 | 16.96 | 11.0 | 7.3 | |
Aloe-emodin | 2,900.00 | 3,012.06 | 9.3 | 2,987.48 | 3.6 | 2,876.80 | −0.8 | 12.9 |
362.50 | 356.72 | 4.1 | 325.67 | 2.2 | 362.14 | −0.1 | 2.7 | |
12.79 | 11.64 | 6.3 | 10.44 | 11.1 | 12.78 | −0.1 | 2.0 | |
Physcion | 6,550.00 | 6,618.43 | 3.3 | 6,667.23 | 2.9 | 7,015.05 | 7.1 | 4.2 |
409.38 | 419.55 | 10.9 | 431.57 | 10.4 | 468.33 | 14.4 | 6.2 | |
12.79 | 13.65 | 13.2 | 10.49 | 14.3 | 13.35 | 4.4 | 1.5 | |
E-glu | 6,350.00 | 6,354.33 | 2.0 | 6,025.67 | 1.3 | 6,464.30 | 1.8 | 4.6 |
396.88 | 396.16 | 4.2 | 405.48 | 4.3 | 359.97 | −9.3 | 3.7 | |
12.40 | 11.22 | 5.5 | 12.19 | 6.1 | 13.22 | 6.6 | 2.8 | |
P-glu | 1,233.30 | 1,227.31 | 2.1 | 1,373.63 | 2.0 | 1,139.57 | −7.6 | 3.3 |
205.50 | 208.37 | 5.1 | 208.73 | 7.4 | 212.28 | 3.3 | 5.2 | |
12.84 | 12.42 | 3.9 | 12.92 | 2.9 | 13.69 | 6.6 | 13.9 | |
Gallic acid | 1,280.00 | 1,272.00 | 3.2 | 1,351.00 | 8.1 | 1,154.56 | −9.8 | 10.2 |
213.32 | 217.25 | 6.1 | 228.94 | 5.3 | 220.79 | 3.5 | 6.3 | |
13.32 | 15.64 | 5.1 | 12.82 | 6.8 | 14.47 | 8.6 | 2.6 | |
Catechin | 4,750.00 | 4,707.67 | 6.4 | 4,450.67 | 4.7 | 4,617.00 | −2.8 | 5.3 |
296.87 | 287.48 | 8.6 | 278.82 | 3.4 | 299.24 | 0.8 | 11.6 | |
18.56 | 18.06 | 3.4 | 17.9 | 8.9 | 20.94 | 12.8 | 8.4 | |
Resveratrol | 8,600.00 | 8,584.83 | 2.9 | 8,545.67 | 2.3 | 9,571.80 | 10.9 | 6.0 |
537.50 | 550.09 | 2.6 | 569.86 | 1.7 | 539.65 | −3.0 | 6.5 | |
16.78 | 17.50 | 5.8 | 17.00 | 6.7 | 15.49 | −3.6 | 5.7 |