TABLE 7.
The results of stability.
| Component | Concentration (ng/ml) | Room temperature 24 h(ng/mL) | RSD (%) | 4°C24h (ng/ml) | RSD (%) | Freeze-thaw (ng/ml) | RSD (%) | Long stability (ng/ml) | RSD (%) |
|---|---|---|---|---|---|---|---|---|---|
| TSG | 14,825.00 | 14,588.47 | 1.9 | 14,393 | 9.7 | 13,676.34 | 5.0 | 14,032.10 | 4.2 |
| 741.25 | 707.81 | 5.1 | 735.65 | 1.3 | 799.25 | 3.2 | 735.67 | 9.0 | |
| 14.83 | 12.23 | 4.0 | 18.27 | 6.4 | 15.70 | 8.4 | 16.57 | 10.1 | |
| Emodin | 38,375.00 | 18,338.88 | 7.9 | 19,254.57 | 5.0 | 16,020.76 | 7.2 | 19,872.84 | 11.6 |
| 767.50 | 783.9 | 6.7 | 773.62 | 2.4 | 703.82 | 11.0 | 723.65 | 9.1 | |
| 15.28 | 15.38 | 3.8 | 12.28 | 7.0 | 17.00 | 9.1 | 12.72 | 5.3 | |
| Aloe-emodin | 2,900.00 | 2,867.01 | 6.1 | 3,021.55 | 2.6 | 3,101.50 | 1.7 | 2,756.34 | 7.8 |
| 362.50 | 375.62 | 10.1 | 325.67 | 9.9 | 408.33 | 1.8 | 357.26 | 8.5 | |
| 12.79 | 11.44 | 12.6 | 10.24 | 8.0 | 9.68 | 5.6 | 13.55 | 2.7 | |
| Physcion | 6,550.00 | 6,258.35 | 10.0 | 6,618.34 | 8.4 | 6,534.22 | 6.3 | 6,896.46 | 11.3 |
| 409.38 | 431.57 | 4.2 | 429.55 | 13.7 | 395.96 | 7.5 | 401.67 | 4.3 | |
| 12.79 | 12.42 | 3.4 | 15.65 | 1.9 | 9.78 | 7.7 | 13.77 | 10.2 | |
| E-glu | 6,350.00 | 6,025.12 | 12.5 | 2054.33 | 11.8 | 6,202.46 | 7.5 | 6,435.66 | 13.9 |
| 396.88 | 366.48 | 8.7 | 366.16 | 2.6 | 409.91 | 10.8 | 394.13 | 12.3 | |
| 12.40 | 13.19 | 6.1 | 15.22 | 9.3 | 11.32 | 11.4 | 11.58 | 11.9 | |
| P-glu | 1,233.30 | 1,129.33 | 7.8 | 1,238.43 | 11.0 | 1,309.48 | 14.9 | 1,286.72 | 4.4 |
| 205.50 | 221.06 | 9.2 | 208.37 | 7.8 | 197.10 | 13.8 | 200.84 | 5.3 | |
| 12.84 | 15.64 | 1.7 | 12.92 | 2.2 | 12.02 | 11.7 | 13.58 | 12.3 | |
| Gallic acid | 1,280.00 | 1,342.38 | 11.9 | 1,272.02 | 13.8 | 1,188.50 | 12.9 | 1,306.35 | 7.9 |
| 213.32 | 278.94 | 4.7 | 277.25 | 12.2 | 199.66 | 7.6 | 201.39 | 8.3 | |
| 13.32 | 13.56 | 11.5 | 12.82 | 8.9 | 11.38 | 4.9 | 14.12 | 6.6 | |
| Catechin | 4,750.00 | 4,650.67 | 4.6 | 4,654.36 | 11.6 | 4,999.10 | 11.6 | 4,726.31 | 6.7 |
| 296.87 | 301.23 | 6.4 | 277.48 | 9.3 | 302.41 | 7.0 | 286.34 | 10.6 | |
| 18.56 | 18.06 | 9.7 | 17.90 | 4.2 | 18.6 | 2.9 | 20.9 | 5.2 | |
| Resveratrol | 8,600.00 | 8,738.41 | 6.8 | 8,654.18 | 1.4 | 8,399.20 | 11.5 | 8,513.48 | 2.4 |
| 537.50 | 521.81 | 4.4 | 542.29 | 1.9 | 501.81 | 6.6 | 514.25 | 1.5 | |
| 16.78 | 16.28 | 8.8 | 15.64 | 8.8 | 18.84 | 7.3 | 15.34 | 6.7 |