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. 2021 May 6;60(24):13380–13387. doi: 10.1002/anie.202101496

Scheme 4.

Scheme 4

a) RP‐HPLC‐ESI‐TOF‐MS of glycoforms IL‐63IL‐69 using acetonitrile/water + 0.1 % HCOOH gradients. b) direct injections of desalted IL‐63IL‐69 (plain water) into ESI‐TOF mass spectrometer show gaussian distribution of charge states; c) overlay of the CD‐spectra of glycosylated IL‐63IL‐69, d) SDS‐PAGE of glycoforms IL‐61IL‐69 (here termed 19).