Scheme 2.
Reaction of 1/2 with [(Cp′′′Co)2(μ,η4:η4‐C7H8)] to the heterobimetallic triple‐decker complexes 3/4; reduction to [K(thf)0.7][5]/[K(thf)0.8][6] and complexation with 18‐c‐6 (Cp′′′=1,2,4‐tri‐tert‐butylcyclopentadienyl).
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