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Molecular structure of the unprecedented products 3 a (left), 4 (middle) and 5 (right). Anisotropic displacement is set to the 50 % probability level. The Cp ligands as well as the CO substituents are drawn translucent and the disorder is omitted for clarity. Selected bond lengths [Å]: 3 a: As−Sb 2.515(1), Mo1‐Mo1′ 3.0656(6); 4: As−Bi 2.64(2), Mo1‐Mo2 3.084(2); 5: Sb−Bi 2.7916(2), Mo1‐Mo1′ 3.1255(6).
