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a) Reaction scheme for the (partial) oxidation of a near‐monodisperse PGEO5MA37 precursor in aqueous solution using NaIO4 at 22 °C. Adjusting the NaIO4/cis‐diol molar ratio (x) between 0.1 and 1.0 generates a library of aldehyde‐functional water‐soluble statistical copolymers. b) Offset 1H NMR spectra (D2O) recorded for PGEO5MA37, P(GEO5MAn‐stat‐AGEO5MAm)37 (where m=0.11, 0.49 and 0.78), and PAGEO5MA37.
