Table 8.
Contents of 6 dianthrones in 86 batches of Polygoni Multiflori Radix Praeparata (PMRP)
| Sample no. | Contents of analytes (µg/g, n = 2a) | ||||||
|---|---|---|---|---|---|---|---|
| 1 | 2 | 3 | 4 | 5 | 6 | Total | |
| Mean ± (SD%)c | Mean ± (SD%)c | Mean ± (SD%)c | Mean ± (SD%)c | Mean ± (SD%)c | Mean ± (SD%)c | ||
| PMRP-01 | 0.60 ± 1.32 | 3.36 ± 1.60 | 0.76 ± 1.04 | 2.57 ± 5.40 | 2.41 ± 6.96 | 2.16 ± 5.87 | 11.86 |
| PMRP-02 | 0.051 ± 0.56 | 0.070 ± 0.98 | 0.064 ± 0.61 | 0.069 ± 0.73 | 0.41 ± 1.10 | 0.36 ± 0.74 | 1.02 |
| PMRP-03 | 0.25 ± 0.42 | 0.45 ± 1.68 | 0.26 ± 1.15 | 0.60 ± 0.79 | 4.50 ± 12.09 | 3.38 ± 5.03 | 9.44 |
| PMRP-04 | 0.051 ± 0.04 | 0.078 ± 0.15 | 0.071 ± 0.26 | 0.11 ± 0.59 | 0.35 ± 0.66 | 0.36 ± 0.78 | 1.02 |
| PMRP-05 | 0.17 ± 0.23 | 0.23 ± 0.33 | 0.18 ± 0.11 | 0.35 ± 0.29 | 7.05 ± 17.31 | 6.70 ± 6.99 | 14.68 |
| PMRP-06 | 0.081 ± 0.25 | 0.071 ± 0.09 | 0.084 ± 0.26 | 0.082 ± 0.17 | 5.47 ± 0.75 | 4.60 ± 17.77 | 10.39 |
| PMRP-07 | 0.12 ± 0.14 | 0.19 ± 0.11 | 0.13 ± 0.11 | 0.28 ± 0.04 | 0.36 ± 0.83 | 0.37 ± 1.62 | 1.45 |
| PMRP-08 | 0.16 ± 0.49 | 0.36 ± 0.70 | 0.19 ± 0.11 | 0.47 ± 0.06 | 7.21 ± 8.07 | 5.10 ± 27.48 | 13.49 |
| PMRP-09 | 0.16 ± 0.09 | 0.47 ± 1.30 | 0.18 ± 0.57 | 0.42 ± 0.48 | 6.30 ± 9.12 | 6.09 ± 18.05 | 13.62 |
| PMRP-10 | 0.079 ± 0.09 | 0.13 ± 0.24 | 0.094 ± 0.02 | 0.17 ± 0.99 | 0.19 ± 0.17 | 0.24 ± 0.61 | 0.90 |
| PMRP-11 | 7.46 ± 2.35 | 5.73 ± 3.87 | 4.23 ± 0.28 | 7.36 ± 4.25 | 9.47 ± 4.41 | 8.05 ± 38.33 | 42.30 |
| PMRP-12 | 0.10 ± 0.06 | 0.34 ± 0.26 | 0.11 ± 0.07 | 0.27 ± 0.19 | 1.25 ± 0.88 | 1.23 ± 2.59 | 3.30 |
| PMRP-13 | 0.030 ± 0.00 | bND | 0.05 ± 0.00 | 0.031 ± 0.00 | 0.098 ± 0.12 | 0.14 ± 0.58 | 0.35 |
| PMRP-14 | 0.090 ± 0.22 | 0.13 ± 0.65 | 0.11 ± 0.40 | 0.16 ± 0.30 | 2.54 ± 1.95 | 2.27 ± 2.78 | 5.30 |
| PMRP-15 | 3.51 ± 4.24 | 3.08 ± 2.97 | 2.47 ± 3.51 | 4.37 ± 9.27 | 2.68 ± 5.17 | 2.12 ± 4.77 | 18.23 |
| PMRP-16 | 0.062 ± 0.05 | 0.095 ± 0.15 | 0.072 ± 0.34 | 0.085 ± 0.17 | 4.08 ± 5.99 | 3.99 ± 3.69 | 8.38 |
| PMRP-17 | 0.070 ± 0.35 | 0.088 ± 0.23 | 0.081 ± 0.02 | 0.10 ± 0.34 | 0.62 ± 2.46 | 0.62 ± 1.38 | 1.58 |
| PMRP-18 | 0.047 ± 0.26 | 0.082 ± 0.37 | 0.067 ± 0.26 | 0.098 ± 0.22 | 0.24 ± 0.20 | 0.27 ± 0.31 | 0.80 |
| PMRP-19 | 4.42 ± 2.17 | 4.67 ± 4.59 | 2.36 ± 5.45 | 6.42 ± 4.79 | 8.68 ± 7.05 | 8.38 ± 28.49 | 34.93 |
| PMRP-20 | 0.51 ± 0.27 | 0.44 ± 0.35 | 0.67 ± 0.15 | 0.64 ± 0.10 | 28.54 ± 7.99 | 25.95 ± 5.23 | 56.75 |
| PMRP-21 | 0.047 ± 0.26 | 0.051 ± 0.19 | 0.074 ± 0.55 | 0.063 ± 0.65 | 0.52 ± 0.61 | 0.45 ± 0.39 | 1.21 |
| PMRP-22 | 0.22 ± 0.12 | 0.29 ± 0.00 | 0.20 ± 0.00 | 0.40 ± 0.32 | 9.31 ± 0.00 | 8.62 ± 0.00 | 19.04 |
| PMRP-23 | 0.030 ± 0.08 | bND | 0.050 ± 0.00 | 0.030 ± 0.45 | 0.19 ± 2.99 | 0.21 ± 2.62 | 0.51 |
| PMRP-24 | 0.77 ± 0.99 | 0.64 ± 0.49 | 0.46 ± 1.93 | 0.99 ± 1.74 | 8.87 ± 10.19 | 8.22 ± 2.72 | 19.95 |
| PMRP-25 | 0.14 ± 0.17 | 0.28 ± 0.44 | 0.18 ± 0.62 | 0.34 ± 0.92 | 2.81 ± 12.24 | 2.02 ± 4.31 | 5.77 |
| PMRP-26 | 0.10 ± 0.06 | 0.068 ± 0.04 | 0.095 ± 0.37 | 0.098 ± 0.11 | 0.71 ± 0.52 | 0.63 ± 1.47 | 1.70 |
| PMRP-27 | 0.26 ± 0.59 | 0.42 ± 0.96 | 0.27 ± 0.02 | 0.67 ± 1.75 | 6.52 ± 5.11 | 5.13 ± 19.97 | 13.27 |
| PMRP-28 | 1.18 ± 0.03 | 1.75 ± 0.53 | 1.35 ± 0.05 | 2.35 ± 0.45 | 13.77 ± 7.12 | 10.30 ± 6.31 | 30.7 |
| PMRP-29 | 0.063 ± 0.11 | 0.14 ± 0.39 | 0.091 ± 0.07 | 0.16 ± 0.52 | 0.95 ± 5.51 | 0.71 ± 2.44 | 2.11 |
| PMRP-30 | 0.054 ± 0.29 | 0.16 ± 0.60 | 0.098 ± 1.79 | 0.12 ± 0.08 | 1.53 ± 3.12 | 1.19 ± 3.69 | 3.15 |
| PMRP-31 | 9.37 ± 8.79 | 6.32 ± 11.82 | 5.23 ± 7.88 | 11.36 ± 14.95 | 8.23 ± 1.64 | 7.79 ± 6.42 | 48.30 |
| PMRP-32 | 3.48 ± 1.90 | 2.02 ± 0.60 | 1.70 ± 1.63 | 3.40 ± 1.31 | 6.73 ± 3.92 | 5.92 ± 22.20 | 23.25 |
| PMRP-33 | 0.065 ± 0.41 | 0.094 ± 0.21 | 0.084 ± 0.28 | 0.12 ± 0.19 | 0.59 ± 5.10 | 0.51 ± 3.46 | 1.46 |
| PMRP-34 | 0.081 ± 0.57 | 0.10 ± 0.58 | 0.085 ± 0.27 | 0.12 ± 0.59 | 0.89 ± 3.39 | 0.70 ± 3.10 | 1.98 |
| PMRP-35 | 0.16 ± 0.81 | 0.23 ± 0.18 | 0.17 ± 0.30 | 0.41 ± 1.48 | 0.32 ± 1.99 | 0.35 ± 1.18 | 1.64 |
| PMRP-36 | 0.15 ± 0.25 | 0.27 ± 0.02 | 0.17 ± 0.07 | 0.34 ± 0.03 | 0.31 ± 0.03 | 3.52 ± 9.47 | 4.76 |
| PMRP-37 | 0.11 ± 0.02 | 0.34 ± 0.14 | 0.12 ± 0.09 | 0.35 ± 0.49 | 0.33 ± 1.51 | 0.31 ± 1.16 | 1.56 |
| PMRP-38 | 0.056 ± 0.01 | 0.075 ± 0.29 | 0.071 ± 0.21 | 0.089 ± 0.01 | 0.28 ± 0.15 | 0.30 ± 1.38 | 0.87 |
| PMRP-39 | 0.21 ± 0.64 | 0.53 ± 0.51 | 0.23 ± 0.15 | 0.59 ± 1.60 | 3.95 ± 12.81 | 2.67 ± 2.57 | 8.18 |
| PMRP-40 | 0.057 ± 0.08 | 0.18 ± 0.83 | 0.072 ± 0.15 | 0.12 ± 0.36 | 3.24 ± 9.23 | 2.66 ± 3.43 | 6.33 |
| PMRP-41 | 0.025 ± 0.29 | 0.051 ± 0.19 | 0.039 ± 0.13 | 0.063 ± 0.31 | 0.38 ± 0.63 | 0.27 ± 0.86 | 0.83 |
| PMRP-42 | bND | 0.089 ± 0.00 | bND | 0.14 ± 0.02 | 0.36 ± 2.36 | 0.24 ± 0.90 | 0.83 |
| PMRP-43 | 0.13 ± 0.028 | 0.39 ± 0.32 | 0.16 ± 1.60 | 0.62 ± 0.53 | 1.42 ± 10.91 | 1.13 ± 14.98 | 3.85 |
| PMRP-44 | 0.025 ± 0.08 | 0.17 ± 0.061 | 0.054 ± 0.13 | 0.23 ± 0.11 | 0.32 ± 0.70 | 0.21 ± 0.15 | 1.01 |
| PMRP-45 | bND | 0.089 ± 0.043 | bND | 0.14 ± 0.00 | 0.33 ± 0.26 | 0.24 ± 0.71 | 0.80 |
| PMRP-46 | 0.028 ± 0.17 | 0.48 ± 0.028 | 0.14 ± 0.37 | 0.56 ± 0.90 | 3.25 ± 16.03 | 3.29 ± 7.35 | 7.86 |
| PMRP-47 | 0.08 ± 0.16 | 0.411 ± 0.08 | 0.073 ± 0.44 | 0.32 ± 0.14 | 0.40 ± 1.05 | 0.28 ± 0.35 | 1.53 |
| PMRP-48 | 0.42 ± 0.04 | 1.63 ± 1.42 | 0.69 ± 0.28 | 2.68 ± 0.31 | 9.86 ± 0.14 | 7.38 ± 1.26 | 22.66 |
| PMRP-49 | 0.20 ± 0.03 | 1.21 ± 0.04 | 0.36 ± 0.00 | 1.59 ± 0.02 | 26.99 ± 10.44 | 27.79 ± 0.27 | 58.14 |
| PMRP-50 | 7.40 ± 2.13 | 5.61 ± 0.37 | 3.94 ± 0.39 | 10.31 ± 1.79 | 11.01 ± 0.97 | 10.85 ± 0.43 | 49.12 |
| PMRP-51 | 0.027 ± 0.38 | 0.13 ± 0.01 | 0.040 ± 0.07 | 0.17 ± 0.18 | 1.90 ± 1.42 | 1.53 ± 0.53 | 3.80 |
| PMRP-52 | 13.03 ± 18.67 | 8.94 ± 20.21 | 7.23 ± 10.11 | 12.75 ± 16.48 | 10.82 ± 61.54 | 12.50 ± 6.99 | 65.27 |
| PMRP-53 | 0.46 ± 0.41 | 1.06 ± 3.01 | 0.54 ± 0.34 | 1.35 ± 3.72 | 1.26 ± 3.35 | 1.41 ± 2.37 | 6.08 |
| PMRP-54 | 0.16 ± 0.08 | 0.54 ± 1.02 | 0.20 ± 0.36 | 0.64 ± 0.52 | 5.29 ± 7.85 | 5.50 ± 14.07 | 12.33 |
| PMRP-55 | 0.072 ± 0.08 | 0.36 ± 0.60 | 0.10 ± 0.03 | 0.41 ± 0.64 | 1.81 ± 4.11 | 1.80 ± 1.06 | 4.55 |
| PMRP-56 | 8.25 ± 4.61 | 4.64 ± 5.20 | 4.95 ± 5.92 | 8.79 ± 10.87 | 3.80 ± 7.98 | 4.60 ± 2.97 | 35.03 |
| PMRP-57 | 0.22 ± 0.78 | 0.58 ± 1.31 | 0.25 ± 0.63 | 0.79 ± 1.61 | 5.18 ± 12.17 | 4.65 ± 3.99 | 11.67 |
| PMRP-58 | 0.40 ± 0.89 | 0.92 ± 4.89 | 0.55 ± 0.53 | 1.15 ± 0.59 | 3.24 ± 0.48 | 3.41 ± 6.09 | 9.67 |
| PMRP-59 | 0.71 ± 0.64 | 0.87 ± 5.14 | 0.54 ± 0.26 | 0.92 ± 1.15 | 16.79 ± 24.06 | 18.91 ± 70.89 | 38.74 |
| PMRP-60 | 5.61 ± 0.64 | 8.19 ± 2.47 | 3.68 ± 0.55 | 10.28 ± 0.99 | 18.71 ± 9.53 | 18.75 ± 7.29 | 65.22 |
| PMRP-61 | 0.032 ± 0.18 | 0.17 ± 0.24 | 0.054 ± 0.23 | 0.21 ± 0.66 | 0.29 ± 2.00 | 0.18 ± 1.71 | 0.94 |
| PMRP-62 | 0.095 ± 0.10 | 0.16 ± 0.75 | 0.069 ± 0.43 | 0.25 ± 0.27 | 0.34 ± 3.00 | 0.24 ± 1.83 | 1.15 |
| PMRP-63 | 0.13 ± 0.07 | 0.57 ± 0.69 | 0.13 ± 0.09 | 0.49 ± 0.13 | 0.56 ± 0.41 | 0.46 ± 1.84 | 2.34 |
| PMRP-64 | bND | 0.12 ± 0.43 | 0.032 ± 0.10 | 0.17 ± 0.48 | 0.26 ± 0.62 | 0.15 ± 0.60 | 0.73 |
| PMRP-65 | 0.028 ± 0.17 | 0.11 ± 0.12 | 0.044 ± 0.04 | 0.17 ± 0.27 | 0.49 ± 0.31 | 0.40 ± 1.86 | 1.24 |
| PMRP-66 | 0.08 ± 0.36 | 0.15 ± 0.10 | 0.040 ± 0.24 | 0.20 ± 1.23 | 0.28 ± 0.09 | 0.19 ± 0.92 | 0.89 |
| PMRP-67 | 0.52 ± 1.64 | 0.36 ± 0.38 | 0.31 ± 0.04 | 0.73 ± 1.15 | 0.38 ± 0.14 | 0.31 ± 0.58 | 2.61 |
| PMRP-68 | bND | 0.090 ± 0.01 | 0.022 ± 0.078 | 0.14 ± 0.080 | 0.31 ± 0.95 | 0.18 ± 0.34 | 0.74 |
| PMRP-69 | 0.028 ± 0.16 | 0.20 ± 0.56 | 0.080 ± 0.03 | 0.27 ± 0.42 | 1.36 ± 2.16 | 1.45 ± 4.49 | 3.41 |
| PMRP-70 | bND | 0.089 ± 0.01 | 0.022 ± 0.019 | 0.14 ± 0.00 | 0.48 ± 0.49 | 0.38 ± 0.40 | 1.11 |
| PMRP-71 | 1.19 ± 4.47 | 0.85 ± 1.93 | 0.89 ± 3.43 | 0.81 ± 4.23 | 2.32 ± 18.15 | 2.21 ± 17.49 | 8.27 |
| PMRP-72 | 0.40 ± 1.45 | 1.21 ± 4.70 | 0.50 ± 0.19 | 1.52 ± 2.72 | 6.52 ± 22.57 | 5.29 ± 18.23 | 15.44 |
| PMRP-73 | 0.45 ± 0.29 | 0.78 ± 1.43 | 0.47 ± 0.79 | 1.21 ± 0.37 | 6.23 ± 10.35 | 5.98 ± 16.38 | 15.12 |
| PMRP-74 | 0.054 ± 0.03 | 0.19 ± 0.53 | 0.059 ± 0.18 | 0.23 ± 0.39 | 3.41 ± 2.97 | 3.25 ± 2.33 | 7.19 |
| PMRP-75 | 0.029 ± 0.14 | 1.25 ± 0.29 | 0.36 ± 0.24 | 1.71 ± 0.16 | 10.67 ± 0.60 | 10.10 ± 1.88 | 24.12 |
| PMRP-76 | 0.55 ± 0.50 | 0.43 ± 0.20 | 0.45 ± 0.81 | 0.51 ± 0.51 | 1.20 ± 0.79 | 1.14 ± 0.16 | 4.28 |
| PMRP-77 | 1.15 ± 1.12 | 0.97 ± 0.54 | 0.98 ± 2.83 | 1.00 ± 0.48 | 6.13 ± 11.15 | 5.36 ± 37.35 | 15.59 |
| PMRP-78 | 1.18 ± 0.21 | 0.95 ± 3.74 | 1.03 ± 0.82 | 0.97 ± 1.22 | 6.23 ± 9.83 | 5.37 ± 15.03 | 15.73 |
| PMRP-79 | 1.34 ± 0.75 | 1.12 ± 2.17 | 1.15 ± 1.72 | 1.08 ± 3.02 | 6.22 ± 5.22 | 5.48 ± 4.66 | 16.39 |
| PMRP-80 | 1.30 ± 0.68 | 0.91 ± 8.23 | 0.90 ± 0.99 | 1.48 ± 1.62 | 1.41 ± 12.83 | 1.44 ± 3.38 | 7.44 |
| PMRP-81 | 0.20 ± 0.39 | 0.47 ± 1.71 | 0.22 ± 0.93 | 0.73 ± 2.19 | 1.73 ± 1.46 | 1.44 ± 3.51 | 4.79 |
| PMRP-82 | bND | 0.090 ± 0.01 | 0.022 ± 0.081 | 0.14 ± 0.12 | 0.38 ± 0.60 | 0.27 ± 0.45 | 0.90 |
| PMRP-83 | 0.19 ± 0.20 | 3.13 ± 1.39 | 1.84 ± 0.42 | 4.48 ± 1.85 | 19.83 ± 2.04 | 21.69 ± 1.97 | 51.16 |
| PMRP-84 | 0.849 ± 1.01 | 1.03 ± 0.79 | 0.76 ± 1.06 | 1.73 ± 3.45 | 5.40 ± 12.61 | 5.86 ± 22.91 | 15.63 |
| PMRP-85 | 0.269 ± 1.38 | 0.51 ± 0.96 | 0.26 ± 0.15 | 0.71 ± 1.08 | 1.38 ± 0.96 | 1.29 ± 0.34 | 4.42 |
| PMRP-86 | 0.65 ± 1.37 | 6.80 ± 1.29 | 3.53 ± 0.35 | 9.55 ± 3.24 | 15.04 ± 3.08 | 15.83 ± 0.01 | 51.40 |
| Average | 0.96 | 1.08 | 0.71 | 1.53 | 4.47 | 4.25 | 12.99 |
aThe data are presented as the average of two replicates
bND, under limits of quantitation
cSD% is presented in the table