. Author manuscript; available in PMC: 2021 Jul 5.

Published in final edited form as: J Am Chem Soc. 2017 Nov 30;139(49):17953–17963. doi: 10.1021/jacs.7b08989

Table 2.

NMR Acquisition Parameters for Double Resonance and Two-Dimensional Experiments Involving ¹⁷O

B₀ (T)	nuclei^a	ω₀/2π (MHz)	pulse sequence	sample	ω_R/2π (kHz)	recycle delay (s)	scans	¹H decouple
17.6	¹H–¹⁷O	749–101.45	R³-R-INEPT	N-Ac-VL	20	0.1	4096	no
	¹⁵N–¹⁷O	76–101.45	REAPDOR	N-Ac-VL	18	3	256	yes
	¹⁵N–¹⁷O	76–101.45	ZF-TEDOR	N-Ac-VL	18	3	60416	yes
21.1	¹³C─¹⁷O	226.3–122.02	ZF-TEDOR	N-Ac-VL	20	3	512	yes
35.2	¹⁷O	203.36	MATPASS	N-Ac-VL	19	0.1	1200	no
			3QMAS		19	0.2	1024	no

Detection nucleus listed first.