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. Author manuscript; available in PMC: 2021 Jul 5.
Published in final edited form as: J Am Chem Soc. 2017 Nov 30;139(49):17953–17963. doi: 10.1021/jacs.7b08989

Table 2.

NMR Acquisition Parameters for Double Resonance and Two-Dimensional Experiments Involving 17O

B0 (T) nucleia ω0/2π (MHz) pulse sequence sample ωR/2π (kHz) recycle delay (s) scans 1H decouple
17.6 1H–17O 749–101.45 R3-R-INEPT N-Ac-VL 20 0.1 4096 no
15N–17O 76–101.45 REAPDOR N-Ac-VL 18 3 256 yes
15N–17O 76–101.45 ZF-TEDOR N-Ac-VL 18 3 60416 yes
21.1 13C─17O 226.3–122.02 ZF-TEDOR N-Ac-VL 20 3 512 yes
35.2 17O 203.36 MATPASS N-Ac-VL 19 0.1 1200 no
3QMAS 19 0.2 1024 no
a

Detection nucleus listed first.