Table 3.

NMR Acquisition Parameters for One- and Two-Dimensional ¹H, ¹³C, and ¹⁵N Experiments

B0 (T)	nucleusa	ω0/2π (MHz)	pulse sequence	sample	ωR/2π (kHz)	recycle delay (s)	scans	1H decouple
11.7	13C	125.3	CP MAS	FMOC-l-leucine	10	3	21280	yes
	13C	125.3	CP MAS	FMOC-l-valine	10	3	18560	yes
	13C	125.3	RFDR	N-Ac-VL	10	3	16	yes
	13C─15N	125.3–50.5	ZF-TEDOR	N-Ac-VL	10	3	256	yes
18.8	1H	800	Bloch decay	N-Ac-VL	60	3	32	no
21.1	1H	900.1	Bloch decay	N-Ac-VL	20	3	16	no
	13C	226.3	CP MAS	N-Ac-VL	20	3	64	yes
	15N	91.2	CP MAS	N-Ac-VL	20	3	256	yes

^aDetection nucleus listed first.