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. 2021 Jun 22;26(13):3785. doi: 10.3390/molecules26133785

Table 1.

Gradient conditions.

Hexane EtoAc EtOH Time (min)
From 0% To 100% 30.2
100% 15
From 0% To 100% 15
100% 15

EtoAc, ethyl acetate; EtOH, ethanol.