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. 2021 Apr 4;82(7):883–895. doi: 10.1002/ddr.21814

SCHEME 4.

SCHEME 4

Synthesis of key starting material 8 (route 2). aReagents and Conditions. a. Amberlyst 15/Lewatit S100, 15–30 °C; b. Electrochemical oxidation, MTBS, 1 atm