TABLE 1.
Crystallographic data collection and refinement statistics
| Parametera | Value(s) for OC43 nsp10:nsp16b |
|---|---|
| PDB accession code | 7NH7 |
| Data collection and processing | |
| Space group | P31 |
| Cell dimensions—a, b, c (Å) | 61.9, 61.9, 109.7 |
| X-ray source | Home source |
| Wavelength (Å) | 1.5419 |
| Resolution range (Å) | 36.57–2.2 (2.28–2.2) |
| No. of unique reflections | 23,828 (2,385) |
| Completeness (%) | 99.74 (99.13) |
| Multiplicity | 5.1 (4.7) |
| Mean I/σ〈I〉 | 11.66 (2.48) |
| CC1/2 | 0.981 (0.687) |
| CC* | 0.995 (0.902) |
| Rmerge (%) | 13.05 (62.57) |
| Structure solution and refinement | |
| Rwork (%) | 16.41 (21.51) |
| Rfree (%) | 21.01 (29.29) |
| RMSD bond length (Å)/bond angle (°) | 0.005/0.86 |
| Avg B factors (Å2) | 28.24 |
| Clashscore | 7.84 |
| Ramachandran plot—favored regions/outlier regions (%) | 97.32/0 |
a
CC1/2, correlation of one half of the observations with the other half; CC*, correlation of the observed data with the unknown “true” intensities.
b
Numbers in parentheses refer to the highest-resolution shell.