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. 2021 Mar 9;60(7):4733–4743. doi: 10.1021/acs.inorgchem.0c03683

Figure 2.

Figure 2

Molecular structure of 1 (a): Thermal ellipsoids at 50% probability; H atoms omitted for clarity. Selected bond distances (Å) and angles (deg): Sb1–C1 2.356(3); Sb1–Cl1 2.8006(8); Sb1–Cl1′ 3.9544(10); Sb1–C18 2.168(3); Sb1–C12 2.171(4). C18–Sb1–C12 102.19(14); C18–Sb1–C1 87.58(12); C12–Sb1–C1 86.33(12); C18–Sb1–Cl1 87.00(8); C12–Sb1–Cl1 85.24(9); C1–Sb1–Cl1 168.80(9). Molecular structure of 2 (b): Thermal ellipsoids at 50% probability; H atoms were omitted for clarity. Selected bond distances (Å) and angles (deg): Bi1–C1 2.489(6); Bi1–Cl1 2.8696(16); Bi1–Cl1′ 3.7211(17); Bi1–C18 2.257(6); Bi1–C12 2.267(6). C18–Bi1–C12 99.0(2); C18–Bi1–C1 86.3(2); C12–Bi1–C1 88.1(2); C18–Bi1–Cl1 86.26(16); C12–Bi1–Cl1 88.26(16); C1–Bi1–Cl1 171.05(15).