Table 4.
Accuracy and precision of TP and PF in plasma (n = 6).
| Analyses | Spiked concentration (ng·mL−1) | Intraday | Interday | ||||
|---|---|---|---|---|---|---|---|
| Found concentration (mean ± SD) | Precision (RSD, %) | Accuracy (RE, %) | Found concentration (mean ± SD) | Precision (RSD, %) | Accuracy (RE, %) | ||
| Triptolide | 15 | 13.25 ± 0.74 | 5.62 | −11.66 | 14.01 ± 0.74 | 5.31 | −6.59 |
| 50 | 55.91 ± 6.64 | 11.87 | 11.82 | 56.36 ± 2.21 | 3.92% | 12.71 | |
| 400 | 376.67 ± 37.69 | 10.01 | −5.83 | 386.97 ± 37.69 | 9.74 | −3.26 | |
|
| |||||||
| Paeoniflorin | 300 | 302.48 ± 19.80 | 6.55 | 0.83 | 303.40 ± 22.21 | 7.32 | 1.13 |
| 10000 | 10513.17 ± 1088.58 | 10.35 | 5.13 | 10488.17 ± 1066.05 | 10.16 | 4.88 | |
| 90000 | 89246.50 ± 9568.47 | 10.72 | −0.84 | 87496.50 ± 10240.51 | 11.70 | −2.78 | |