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. 2021 Jul 15;11:14539. doi: 10.1038/s41598-021-93285-7

Table 1.

Physicochemical characteristics of the isolated compounds K1 and K2.

Physicochemical characteristics Isolated compounds
K1 K2
Color and appearance Reddish-orange amorphous Reddish-orange amorphous
Solubility

Highly soluble: chloroform, ethyl acetate, dichloromethane, acetonitrile, methanol, acetone

Partial-soluble: ethanol, dimethylformamide, dimethyl sulphoxide, water

Non-soluble: n-hexane

Highly soluble: chloroform, ethyl acetate, dichloromethane, acetonitrile, methanol, acetone

Partial-soluble: ethanol, dimethylformamide, dimethyl sulphoxide, water

Non-soluble: n-hexane

Melting point (°C) 245–250 with decomposition 245–250 with decomposition
UV–Visible (λmax, nm) 239, 440 (Methanol) 215, 442 (Methanol)
FT-IR (υmax, cm-1)

1583 (N–H bending)

1648–1668 (C=C stretching)

1705–1740 (C=O stretching)

2849–2916 (C–H stretching)

1587 (N–H bending)

1627–1656 (C=C stretching)

1728 (C=O stretching)

2853–2957 (C–H stretching)

( +)-HR-ESI-MS m/z 1269.6170 [M + H]+ (calcd for C62H85N12O17, 1269.616); m/z 1291.5997 [M + Na]+ (calcd for C62H84N12O17Na, 1291.598) m/z 1255.638 [M + H]+ (calcd. for C62H87N12O16, 1255.637); 1277.623 [M + Na]+ (calcd. for C62H86N12O16Na, 1277.619)
Monoisotopic masses 1268.617 g/mol 1254.638 g/mol