Table 1.
Physicochemical characteristics of the isolated compounds K1 and K2.
Physicochemical characteristics | Isolated compounds | |
---|---|---|
K1 | K2 | |
Color and appearance | Reddish-orange amorphous | Reddish-orange amorphous |
Solubility |
Highly soluble: chloroform, ethyl acetate, dichloromethane, acetonitrile, methanol, acetone Partial-soluble: ethanol, dimethylformamide, dimethyl sulphoxide, water Non-soluble: n-hexane |
Highly soluble: chloroform, ethyl acetate, dichloromethane, acetonitrile, methanol, acetone Partial-soluble: ethanol, dimethylformamide, dimethyl sulphoxide, water Non-soluble: n-hexane |
Melting point (°C) | 245–250 with decomposition | 245–250 with decomposition |
UV–Visible (λmax, nm) | 239, 440 (Methanol) | 215, 442 (Methanol) |
FT-IR (υmax, cm-1) |
1583 (N–H bending) 1648–1668 (C=C stretching) 1705–1740 (C=O stretching) 2849–2916 (C–H stretching) |
1587 (N–H bending) 1627–1656 (C=C stretching) 1728 (C=O stretching) 2853–2957 (C–H stretching) |
( +)-HR-ESI-MS | m/z 1269.6170 [M + H]+ (calcd for C62H85N12O17, 1269.616); m/z 1291.5997 [M + Na]+ (calcd for C62H84N12O17Na, 1291.598) | m/z 1255.638 [M + H]+ (calcd. for C62H87N12O16, 1255.637); 1277.623 [M + Na]+ (calcd. for C62H86N12O16Na, 1277.619) |
Monoisotopic masses | 1268.617 g/mol | 1254.638 g/mol |