Table 3.
Inter- and intraday precision and accuracy for the analytes in human plasma.
| Analytes | Concentration (ng/mL)a | Intra-day |
Inter-day |
||||
|---|---|---|---|---|---|---|---|
| Measured concentration (ng/mL) | Precision (%) | Accuracy (%) | Measured concentration (ng/mL) | Precision (%) | Accuracy (%) | ||
| INH | 48 | 45.93 | 7.18 | 95.71 | 45.28 | 6.91 | 94.36 |
| 120 | 118.83 | 3.17 | 98.98 | 121.50 | 4.01 | 101.28 | |
| 1920 | 2003.33 | 3.62 | 104.36 | 1956.67 | 4.88 | 101.89 | |
| 4800 | 5003.33 | 3.18 | 104.22 | 4874.44 | 3.24 | 101.59 | |
| RIF | 200 | 207.67 | 11.68 | 103.80 | 189.78 | 12.11 | 94.91 |
| 500 | 532.50 | 6.71 | 106.49 | 524.06 | 7.65 | 104.83 | |
| 8000 | 8831.67 | 4.38 | 110.40 | 8210.56 | 7.27 | 102.64 | |
| 20000 | 21633.33 | 7.37 | 108.22 | 20200 | 7.14 | 100.99 | |
| EMB | 96 | 86.68 | 8.43 | 90.30 | 84.85 | 6.81 | 88.38 |
| 240 | 236.33 | 4.17 | 98.36 | 239.11 | 4.69 | 99.61 | |
| 3840 | 4023.33 | 3.24 | 104.77 | 3900 | 4.19 | 103.89 | |
| 9600 | 10030 | 4.70 | 104.58 | 9650 | 7.27 | 100.55 | |
| PZA | 480 | 482.67 | 8.14 | 100.54 | 457.78 | 7.43 | 95.34 |
| 1200 | 1238.33 | 2.67 | 103.22 | 1226.11 | 5.07 | 102.16 | |
| 19200 | 19566.67 | 3.29 | 101.92 | 19288.89 | 2.81 | 100.46 | |
| 48000 | 47816.67 | 1.80 | 99.61 | 47927.78 | 2.80 | 99.85 | |
| AC-INH | 192 | 201.33 | 11.63 | 104.91 | 188.56 | 10.21 | 98.23 |
| 480 | 476.17 | 5.32 | 99.20 | 480.50 | 5.70 | 100.13 | |
| 7680 | 8001.67 | 5.29 | 104.20 | 7829.44 | 4.42 | 101.94 | |
| 19200 | 19300 | 4.16 | 100.51 | 19188.89 | 2.97 | 99.96 | |
The QC samples from top to bottom are the LLOQ, LQC, MQC, and HQC.