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Electrochemical reduction of nitroarenes to azo-aromatics over a CoP cathodea.
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aNitro substrates (0.5 mmol), CoP (working area: 1 cm2), 1.0 M KOH (25 mL), room temperature, −0.75 V and then turned to −1.1 V vs. Ag/AgCl. Con. is the abbreviation for conversion and sel. for selectivity. The con. and sel. are determined by gas chromatography.
