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. 2021 Jun 15;3(7):3438–3445. doi: 10.1021/acsapm.1c00378

Table 1. Quantities Used in Cures.

amine mass (amine) (g) moles (amine) (mol) epoxy mass (epoxy) (g) moles (epoxy) (mol) stoich pot time (h)
MXDA 2.2584 6.63 × 10–2 DER354 11.2228 6.63 × 10–2 100.0% 3
1,3-BAC 2.8368 7.98 × 10–2 DER354 13.4864 7.97 × 10–2 100.1% 2
PXDAa 2.9875 8.77 × 10–2 DER354 14.8443 8.77 × 10–2 100.0% 1.25
1,4-BAC 2.1566 6.06 × 10–2 DER354 10.2604 6.06 × 10–2 100.0% 2
MXDA 2.7971 8.22 × 10–2 E828 15.4733 8.21 × 10–2 100.0% 2.5
MXDA 3.0718 9.02 × 10–2 PY306 15.0585 9.02 × 10–2 100.0% 3
MXDA 2.8835 8.47 × 10–2 DER332 14.7063 8.46 × 10–2 100.0% 2.5
a

PXDA is a solid hardener, and therefore, the pot was held at an elevated temperature (30 °C) in order to reduce the likelihood of crystallization.