Table 1.
Solvent | Conversion (%) | ||
---|---|---|---|
CALB | CALA | BCL | |
Toluene | 92 | 76 | 5 |
ChCl:Acetamide (1:2) | 96 | 0.5 | 0 |
ChCl:Glycerol (1:2) | 96 | 70 | 22 |
ChCl:Malonate (1:1) | 58 | 0.7 | 0 |
ChCl:Urea (1:2) | 99 | 1.6 | 0.8 |
EAC:Acetamide (2:3) | 92 | 2.7 | 0 |
EAC:Glycerol (2:3) | 91 | 2.1 | 0.5 |
Reaction is shown in Figure 3a; conditions: 60 °C, 24 h. ChCl = choline chloride, EAC = ethylammonium chloride