Table 7.
X-ray powder diffraction crystal data of complexes.
| Parameters | Ni(II) complex | Cu(II) complex | Mn(II) complex | Fe(II) complex |
|---|---|---|---|---|
| Empirical formula | C32H36N2NiP2O2Cl2 | C32H34N2CuP2OCl2 | C32H34N2MnP2OCl2 | C32H38N2FeP2O3Cl2 |
| Formula weight | 672.2 | 659.02 | 650.41 | 687.38 |
| Crystal system | Triclinic | Monoclinic | Triclinic | Monoclinic |
| a (Å) | 15.509 | 13.140 | 15.503 | 11.491 |
| b (Å) | 16.785 | 9.857 | 16.788 | 7.393 |
| c (Å) | 10.223 | 6.018 | 10.224 | 9.781 |
| Alfa (°) | 103.303 | 90.00 | 103.295 | 90.00 |
| Beta (°) | 96.349 | 103.20 | 96.342 | 117.25 |
| gamma (°) | 105.685 | 90.00 | 105.656 | 90.00 |
| Volume of unit cell (Å3) | 2450.6 | 758.99 | 2450.9 | 738.7 |