Table 1.
Feedstock | Method | Length (nm) | Width (nm) | CrI (%) | Yield (%) | Carboxyl Content (mmol/g) | Ref. |
---|---|---|---|---|---|---|---|
Cotton linters | HCl, TEMPO | n.r. | 4–5 | 75 | 81 | 0.15 (DO) | [22] |
Sugar beet pulp | HCl, TEMPO | n.r. | 3–4 | 52 | 63 | 0.23 (DO) | [22] |
Softwood-bleached kraft pulp | TEMPO, cavitation | 155–244 | 3.6 | 81 | 94 | 1.57 | [24] |
MCC | TEMPO, cavitation | 163–192 | 4.3 | 88 | 70 | 1.12 | [24] |
Flax fibers | APS | 144 ± 5 | 3.8 ± 0.1 | 75 | 28 | 0.18 (DO) | [20] |
Flax shives | APS | 296 ± 16 | 5.1 ± 0.1 | 64 | 22 | 0.19 (DO) | [20] |
Hemp fibers | APS | 148 ± 3 | 5.8 ± 0.1 | 73 | 36 | 0.17 (DO) | [20] |
Triticale straw extract | APS | 134 ± 5 | 4.2 ± 0.1 | 73 | 31 | 0.11 (DO) | [20] |
MCC | APS | 128 ± 4 | 5.5 ± 0.1 | 83 | 65 | 0.19 (DO) | [20] |
Whatman CF1 | APS | 121 ± 3 | 6.7 ± 0.3 | 91 | 81 | 0.12 (DO) | [20] |
Wood pulp | APS | 124 ± 6 | 6.0 ± 0.2 | 81 | 36 | 0.19 (DO) | [20] |
Bacterial cellulose | APS | 88 ± 5 | 6.5 ± 0.2 | 70 | 14 | 0.14 (DO) | [20] |
Black spruce dissolving pulp | H2O2 | 170 | 10 | n.r. | n.r. | 0.15 | [21,65] |
Dissolving pulp | NaOCl, transition metal catalyzed | 100–150 | 9–14 | 80 | n.r. | 0.15 | [49] |
Lemon seed | APS | 140–160 | 10–20 | 74 | 13 | n.r. | [41] |
Lemon seed | TEMPO | 340–380 | 26–42 | 66 | 52 | n.r. | [41] |
Juncus plant | Citric acid/HCl | 352 ± 79 | 6.1 ± 2.8 | 83 | n.r. | n.r. | [58] |
Tomato plant residues | Citric acid/HCl | 514 ± 131 | 4.7 ± 1.4 | 78 | n.r. | n.r. | [59] |
Bamboo borer powder | APS | 20–50 (spheres) | - | 63 | n.r. | n.r. | [42] |
Recycled paper | APS | 130 ± 15 | 4.7 ± 2.5 | 72 | 22 | 0.57 | [40] |
Tunicate | APS | 383 ± 164 | 10.9 ± 2.3 | 86 | n.r. | 0.07 (DO) | [44] |
Cotton powder | APS, microwave | 80–400 | 7 | n.r. | 46 | n.r. | [39] |
Softwood pulp | TEMPO | 103 ± 29 | 21 ± 7 | n.r. | 12 | 0.7 | [66] |
Softwood pulp | Cu2SO4/H2O2 | 247 ± 58 | 6 ± 2 | n.r. | 51 | 0.9 | [66] |
Cotton pulp | APS/TMEDA | 80–350 | 3–12 | 91 | 63 | 1.38 | [37] |
Cotton pulp | H2SO4, KMnO4/oxalic acid | 150–300 | 10–22 | 89 | 68 | 1.58 | [51] |
MCC | H2SO4, HNO3 | 186 ± 13 | 9 ± 3 | 91 | 24 | 0.11 | [52] |
Sugarcane bagasse | Citric acid, ultrasonication | 251 ± 52 | 21 ± 6 | 77 | 32 | 0.60 | [55] |
MCC | Citric acid, HCl | 231.8 ± 23.2 | 15.8 ± 3.0 | 83 | 88 | 1.40 | [56] |
Bleached eucalyptus kraft pulp | Citric acid, FeCl3 | 100–250 | 6–12 | 80 | 80 | 0.90 | [60] |
Bleached eucalyptus kraft pulp | Oxalic acid | 278 | 19 | 81 | 25 | 0.19 | [53] |
Softwood pulp | Sodium periodate, sodium chlorite | 120–200 | 13 | 91 | n.r. | 6.6 | [61] |
Bleached kraft pulp | H2SO4, sodium chlorite, 4% hypochlorite | 150–200 | 5–20 | n.r | 50 | n.r | [67] |
Elephant grass | TEMPO, ultrasonication | 174 ± 73 | 5.2 ± 1.4 | n.r | n.r | n.r. | [32,33] |
Bleached kraft pulp | LiBr/H2SO4, APS | 57 ± 24 | 9.3 ± 3.1 | 96 | 52 | 0.44 | [45] |
Recycled medium-density fiberboard | APS | 170–365 | 13–17 | 63 | 55 | 0.10 (DO) | [46] |
Denim waste | NaOH, APS | 81.5 ± 20.5 | 18.4 ± 2.5 | 27 | 79 | n.r. | [47] |
Balsa fibers | APS | 95.5 | 6.5 | n.r. | 57.7 | n.r. | [48] |
Kapok fibers | APS | 112.1 | 5.8 | n.r. | 60.7 | n.r. | [48] |
n.r. = not reported; DO: degree of oxidation.