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. 2021 Jun 22;11(7):1641. doi: 10.3390/nano11071641

Table 1.

Production of cCNCs from different feedstock materials.

Feedstock Method Length (nm) Width (nm) CrI (%) Yield (%) Carboxyl Content (mmol/g) Ref.
Cotton linters HCl, TEMPO n.r. 4–5 75 81 0.15 (DO) [22]
Sugar beet pulp HCl, TEMPO n.r. 3–4 52 63 0.23 (DO) [22]
Softwood-bleached kraft pulp TEMPO, cavitation 155–244 3.6 81 94 1.57 [24]
MCC TEMPO, cavitation 163–192 4.3 88 70 1.12 [24]
Flax fibers APS 144 ± 5 3.8 ± 0.1 75 28 0.18 (DO) [20]
Flax shives APS 296 ± 16 5.1 ± 0.1 64 22 0.19 (DO) [20]
Hemp fibers APS 148 ± 3 5.8 ± 0.1 73 36 0.17 (DO) [20]
Triticale straw extract APS 134 ± 5 4.2 ± 0.1 73 31 0.11 (DO) [20]
MCC APS 128 ± 4 5.5 ± 0.1 83 65 0.19 (DO) [20]
Whatman CF1 APS 121 ± 3 6.7 ± 0.3 91 81 0.12 (DO) [20]
Wood pulp APS 124 ± 6 6.0 ± 0.2 81 36 0.19 (DO) [20]
Bacterial cellulose APS 88 ± 5 6.5 ± 0.2 70 14 0.14 (DO) [20]
Black spruce dissolving pulp H2O2 170 10 n.r. n.r. 0.15 [21,65]
Dissolving pulp NaOCl, transition metal catalyzed 100–150 9–14 80 n.r. 0.15 [49]
Lemon seed APS 140–160 10–20 74 13 n.r. [41]
Lemon seed TEMPO 340–380 26–42 66 52 n.r. [41]
Juncus plant Citric acid/HCl 352 ± 79 6.1 ± 2.8 83 n.r. n.r. [58]
Tomato plant residues Citric acid/HCl 514 ± 131 4.7 ± 1.4 78 n.r. n.r. [59]
Bamboo borer powder APS 20–50 (spheres) - 63 n.r. n.r. [42]
Recycled paper APS 130 ± 15 4.7 ± 2.5 72 22 0.57 [40]
Tunicate APS 383 ± 164 10.9 ± 2.3 86 n.r. 0.07 (DO) [44]
Cotton powder APS, microwave 80–400 7 n.r. 46 n.r. [39]
Softwood pulp TEMPO 103 ± 29 21 ± 7 n.r. 12 0.7 [66]
Softwood pulp Cu2SO4/H2O2 247 ± 58 6 ± 2 n.r. 51 0.9 [66]
Cotton pulp APS/TMEDA 80–350 3–12 91 63 1.38 [37]
Cotton pulp H2SO4, KMnO4/oxalic acid 150–300 10–22 89 68 1.58 [51]
MCC H2SO4, HNO3 186 ± 13 9 ± 3 91 24 0.11 [52]
Sugarcane bagasse Citric acid, ultrasonication 251 ± 52 21 ± 6 77 32 0.60 [55]
MCC Citric acid, HCl 231.8 ± 23.2 15.8 ± 3.0 83 88 1.40 [56]
Bleached eucalyptus kraft pulp Citric acid, FeCl3 100–250 6–12 80 80 0.90 [60]
Bleached eucalyptus kraft pulp Oxalic acid 278 19 81 25 0.19 [53]
Softwood pulp Sodium periodate, sodium chlorite 120–200 13 91 n.r. 6.6 [61]
Bleached kraft pulp H2SO4, sodium chlorite, 4% hypochlorite 150–200 5–20 n.r 50 n.r [67]
Elephant grass TEMPO, ultrasonication 174 ± 73 5.2 ± 1.4 n.r n.r n.r. [32,33]
Bleached kraft pulp LiBr/H2SO4, APS 57 ± 24 9.3 ± 3.1 96 52 0.44 [45]
Recycled medium-density fiberboard APS 170–365 13–17 63 55 0.10 (DO) [46]
Denim waste NaOH, APS 81.5 ± 20.5 18.4 ± 2.5 27 79 n.r. [47]
Balsa fibers APS 95.5 6.5 n.r. 57.7 n.r. [48]
Kapok fibers APS 112.1 5.8 n.r. 60.7 n.r. [48]

n.r. = not reported; DO: degree of oxidation.