Table 3.
Percentage content of crude and fractions from liquid chromatograph-mass spectrometry.
| Crude/fraction | RT/min | % content | Some fragment ions |
|---|---|---|---|
| C1 | 1.839 | 100 | 101.0, 146.1, 179.1, 241.1, 319.1, 373.1 |
| C2 | 1.846 | 100 | 101.1, 146.1, 179.1, 202.3, 241.1, 319.1, 373.1 |
| C3 | 1.846 | 100 | 101.1, 146.1, 179.1, 241.1, 319.1, 373.1 |
| C5 | 1.846 | 100 | 101.1, 146.1, 179.1, 202.3, 241.1, 319.1, 373.1 |
| C6 | 1.839 10.145 |
87.3 12.7 |
101.1, 146.1, 179.1, 241.1, 319.1, 373.1 111.1, 161.2, 210.2, 261.2, 349.2, 397.3, 535.1 |
| C7 | 1.372 1.595 1.839 10.145 |
10.28 6.35 79.68 9.69 |
111.1, 161.2, 223.1, 245.2, 263.2, 349.2, 393.2 89.1, 111.1, 161.2, 203.1, 245.2, 290.2, 349.2, 383.2, 435.1 101.0, 146.1, 179.1, 241.1, 319.1, 373.0 111.1, 161.2, 210.2, 261.2, 349.2, 397.3, 535.0 |
| C8 | 1.609 1.861 |
24.38 74.62 |
111.1, 161.1, 203.1, 290.2, 349.2, 383.2, 445.2 101.0, 146.1, 179.0, 241.1, 319.1, 373.0, 533.4 |
| Crude extract | 1.853 | 100 | 101.1, 111.1, 161.1, 163.1, 205.1, 223.1, 261.1, 279.2 349.2, 535.0 |
RT: retention time.