Table 1. Melting Points, Yield Percentages, Molecular Formulae, and Molecular Weights of Compounds 8, 10–21, 23, 24, and 26–33.
comp. no. | R | R′/Ar | melting point (°C) | yield (%) | mol. formula (Mol. Wt.) |
---|---|---|---|---|---|
8 | CH3 | 4-CH3C6H4 | 314–316 | 90 | C21H17N3OS2 (391.51) |
10 | CH3 | 3,4-(CH3O)2C6H3 | 290–292 | 85 | C22H19N3O3S2 (437.53) |
12 | CH3 | 2,4-Cl2C6H3 | 322–325 | 84 | C20H13Cl2N3OS2 (446.37) |
13 | CH3 | thiophen-2-yl | 328–330 | 90 | C18H13N3OS3 (383.51) |
14 | CH3 | 5-bromothiophen-2-yl | 320–322 | 86 | C18H12BrN3OS3 (462.41) |
15 | OCH3 | 4-CH3C6H4 | 308–310 | 90 | C21H17N3O2S2 (407.51) |
16 | OCH3 | 4-CH3OC6H4 | 322–325 | 90 | C21H17N3O3S2 (423.51) |
17 | OCH3 | 3,4-(CH3O)2C6H3 | 293–295 | 80 | C22H19N3O4S2 (453.53) |
18 | OCH3 | 4-ClC6H4 | 325–328 | 80 | C20H14ClN3O2S2 (427.93) |
19 | OCH3 | 2,4-Cl2C6H3 | 328–330 | 90 | C20H13Cl2N3O2S2 (462.37) |
20 | OCH3 | thiophen-2-yl | 325–327 | 80 | C18H13N3O2S3 (399.51) |
21 | OCH3 | 5-bromothiophen-2-yl | 288–290 | 80 | C18H12BrN3O2S3 (478.41) |
23 | 335–338 | 65 | C22H16N4O4S2 (464.52) | ||
24 | CH3 | CH3 | 220–222 | 79 | C13H15N3S2 (277.41) |
26 | OCH3 | CH3 | 210–212 | 69 | C13H15N3OS2 (293.41) |
27 | OCH3 | C6H5 | 215–217 | 79 | C18H17N3OS2 (355.48) |
28 | CH3 | CH3 | 208–210 | 64 | C15H15N3OS2 (317.43) |
29 | CH3 | C6H5 | 198–200 | 66 | C20H17N3OS2 (379.5) |
30 | OCH3 | CH3 | 215–215 | 66 | C15H15N3O2S2 (333.43) |
31 | OCH3 | C6H5 | 210–212 | 68 | C20H17N3O2S2 (395.5) |
32 | 3,4-(CH3O)2C6H3 | 217–218 | 79 | C29H25N3O4S2 (543.66) | |
33 | 2,4-Cl2C6H3 | 189–191 | 80 | C27H19Cl2N3O2S2 (552.49) |