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. 2021 Jul 19;6(29):19202–19211. doi: 10.1021/acsomega.1c02549

Table 1. Melting Points, Yield Percentages, Molecular Formulae, and Molecular Weights of Compounds 8, 10–21, 23, 24, and 26–33.

comp. no. R R′/Ar melting point (°C) yield (%) mol. formula (Mol. Wt.)
8 CH3 4-CH3C6H4 314–316 90 C21H17N3OS2 (391.51)
10 CH3 3,4-(CH3O)2C6H3 290–292 85 C22H19N3O3S2 (437.53)
12 CH3 2,4-Cl2C6H3 322–325 84 C20H13Cl2N3OS2 (446.37)
13 CH3 thiophen-2-yl 328–330 90 C18H13N3OS3 (383.51)
14 CH3 5-bromothiophen-2-yl 320–322 86 C18H12BrN3OS3 (462.41)
15 OCH3 4-CH3C6H4 308–310 90 C21H17N3O2S2 (407.51)
16 OCH3 4-CH3OC6H4 322–325 90 C21H17N3O3S2 (423.51)
17 OCH3 3,4-(CH3O)2C6H3 293–295 80 C22H19N3O4S2 (453.53)
18 OCH3 4-ClC6H4 325–328 80 C20H14ClN3O2S2 (427.93)
19 OCH3 2,4-Cl2C6H3 328–330 90 C20H13Cl2N3O2S2 (462.37)
20 OCH3 thiophen-2-yl 325–327 80 C18H13N3O2S3 (399.51)
21 OCH3 5-bromothiophen-2-yl 288–290 80 C18H12BrN3O2S3 (478.41)
23     335–338 65 C22H16N4O4S2 (464.52)
24 CH3 CH3 220–222 79 C13H15N3S2 (277.41)
26 OCH3 CH3 210–212 69 C13H15N3OS2 (293.41)
27 OCH3 C6H5 215–217 79 C18H17N3OS2 (355.48)
28 CH3 CH3 208–210 64 C15H15N3OS2 (317.43)
29 CH3 C6H5 198–200 66 C20H17N3OS2 (379.5)
30 OCH3 CH3 215–215 66 C15H15N3O2S2 (333.43)
31 OCH3 C6H5 210–212 68 C20H17N3O2S2 (395.5)
32   3,4-(CH3O)2C6H3 217–218 79 C29H25N3O4S2 (543.66)
33   2,4-Cl2C6H3 189–191 80 C27H19Cl2N3O2S2 (552.49)