Table 1. Data collection, processing, and refinement.
| TaTT mutants | mP3 | mP3O1 |
|---|---|---|
| Diffraction source | BL41XU, Spring8 | BL41XU, Spring8 |
| Wavelength (Å) | 1.00 | 1.00 |
| Temperature (K) | 100 | 100 |
| Detector | PILATUS | PILATUS |
| Crystal-to-detector distance (mm) | 190.0 | 250.0 |
| Rotation range per image (°) | 0.5 | 1.0 |
| Total rotation range (°) | 100 | 130 |
| Space group | H32 | H32 |
| a, b, c (Å) | 146.50, 146.50, 143.78 | 146.02, 146.02, 142.12 |
| α, β, γ (°) | 90.0, 90.0, 120.0 | 90.0, 90.0, 120.0 |
| Resolution range (Å) | 95.13–1.75 (1.78–1.75) | 94.47–1.90 (1.94–1.90) |
| Completeness (%) | 98.6 (98.2) | 98.8 (99.4) |
| Average redundancy | 2.8 (2.8) | 4.0 (4.0) |
| 〈I/σ(I)〉 | 11.3 (1.0) | 10.0 (0.3) |
| Rmeas (%) (Diederichs and Karplus 1997) | 5.5 (100.1) | 8.3 (440.1) |
| CC1/2 (Diederichs and Karplus 1997) | 99.9 (40.1) | 99.9 (12.1) |
| Rfact (%) | 16.1 | 20.6 |
| Rfree. (%) | 20.1 | 25.5 |
| Bonds (Å) | 0.02 | 0.02 |
| Angles (°) | 2.03 | 2.22 |
| Ramachandran plot | ||
| Most favoured (%) | 96.0 | 93.3 |
| Allowed (%) | 2.6 | 3.9 |
| PDB entry code | 7NEA | 7NEB |