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| USP | Neue Methode | |
|---|---|---|
| Säule | 250 × 4,6 mm (L1 RP-18) |
Nucleodur 100‑3 C18 ec, 150 × 4 mm + Universalvorsäule EC 3/4 |
| Mobile Phase |
Acetonitril: MeOH: H2O 106:55:39 (V/V/V) |
MeOH: H2O: Ameisensäure 93:7:0,1 (V/V/V) |
| Retentionszeit | Ca. 40 min | 5,5 min |
| Druck | 118 bar | 142 bar |
| Flussrate | 1,5 ml/min | 0,8 ml/min |
| Injektionsvolumen | 10 μl | |
| Detektion | UV: 245 nm | |
| Lösungsmittel | MeOH | |
USP United States Pharmacopeia, MeOH Methanol, H2O Wasser
