Table 3. H–D Exchange Reaction of 3-Unsubstituted Indolesa.
Reactions were performed in CD3CO2D (0.1 M) in a sealed tube at 150 °C for 110 h.
D content was calculated based on the 1H NMR spectra of the isolated product.
Isolated yield.
D content was calculated based on 1H NMR spectroscopy after N-methylation.
Indicated as average D incorporation.