Table 2. Experimental details.
| Crystal data | |
| Chemical formula | C15H21NO3 |
| M r | 263.33 |
| Crystal system, space group | Monoclinic, P21/c |
| Temperature (K) | 133 |
| a, b, c (Å) | 18.4574 (8), 5.7020 (2), 14.8058 (6) |
| β (°) | 113.468 (1) |
| V (Å3) | 1429.33 (10) |
| Z | 4 |
| Radiation type | Mo Kα |
| μ (mm−1) | 0.09 |
| Crystal size (mm) | 0.10 × 0.10 × 0.08 |
| Data collection | |
| Diffractometer | Nonius KappaCCD |
| Absorption correction | Multi-scan (SADABS; Krause et al., 2015 ▸) |
| T min, T max | 0.674, 0.746 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 13968, 3280, 2464 |
| R int | 0.040 |
| (sin θ/λ)max (Å−1) | 0.649 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.049, 0.113, 1.04 |
| No. of reflections | 3280 |
| No. of parameters | 177 |
| H-atom treatment | H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) | 0.27, −0.21 |