| Crystal data |
| Chemical formula |
[U13(CH3O)35.7Cl2.3O8] |
|
M
r
|
4412.01 |
| Crystal system, space group |
Triclinic, P\overline{1} |
| Temperature (K) |
100 |
|
a, b, c (Å) |
12.8598 (6), 14.0014 (6), 14.6311 (6) |
| α, β, γ (°) |
117.339 (2), 113.186 (2), 92.373 (2) |
|
V (Å3) |
2069.95 (16) |
|
Z
|
1 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
25.48 |
| Crystal size (mm) |
0.12 × 0.11 × 0.08 |
| |
| Data collection |
| Diffractometer |
Bruker D8 Venture |
| Absorption correction |
Multi-scan (Krause et al., 2015 ▸) |
|
T
min, T
max
|
0.394, 0.746 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
55319, 7304, 6185 |
|
R
int
|
0.052 |
| (sin θ/λ)max (Å−1) |
0.595 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.038, 0.103, 1.09 |
| No. of reflections |
7304 |
| No. of parameters |
488 |
| No. of restraints |
145 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
5.02, −3.41 |
