Table 4. Cell parameters determined from SCXRD and PXRD at different temperatures.
| Compound | PL358 | PL358 | PL358 | SY20C174 | SY20C174 | SY20C174 |
|---|---|---|---|---|---|---|
| XRD measurement | SCXRD | SCXRD | PXRD | SCXRD | SCXRD | PXRD |
| Temperature | 110 K | 295 K | 295 K | 100 K | 298 K | 295 K |
| Space group | P212121 | P212121 | P212121 | P212121 | P212121 | P212121 |
| a | 6.4201 (2) | 6.467 (5) | 6.4775 (2) | 6.0146 (2) | 6.157 (9) | 6.1573 (2) |
| b | 17.6239 (7) | 17.887 (12) | 17.9583 (7) | 19.2817 (7) | 19.46 (3) | 19.4684 (7) |
| c | 20.8997 (8) | 20.897 (15) | 20.9335 (7) | 20.9887 (7) | 20.92 (3) | 20.8859 (9) |
| Volume | 2364.7 (1) | 2417 (5) | 2435.1 (1) | 2434.1 (1) | 2508 (11) | 2503.7 (2) |