Table 7. Experimental details.
| Crystal data | |
| Chemical formula | [Zn(C22H17N4O2S)2] |
| M r | 868.28 |
| Crystal system, space group | Monoclinic, P21/n |
| Temperature (K) | 100 |
| a, b, c (Å) | 13.4029 (4), 15.8310 (4), 19.6257 (6) |
| β (°) | 107.841 (3) |
| V (Å3) | 3964.0 (2) |
| Z | 4 |
| Radiation type | Mo Kα |
| μ (mm−1) | 0.78 |
| Crystal size (mm) | 0.34 × 0.17 × 0.12 |
| Data collection | |
| Diffractometer | Oxford Diffraction Gemini |
| Absorption correction | Multi-scan (CrysAlis PRO; Agilent, 2012 ▸) |
| T min, T max | 0.865, 1.000 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 17644, 8932, 7199 |
| R int | 0.032 |
| (sin θ/λ)max (Å−1) | 0.679 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.036, 0.086, 1.02 |
| No. of reflections | 8932 |
| No. of parameters | 540 |
| No. of restraints | 2 |
| H-atom treatment | H atoms treated by a mixture of independent and constrained refinement |
| Δρmax, Δρmin (e Å−3) | 0.36, −0.40 |