Table 2.

NMR Data From Membranoids F (10),^a G (11),^a and H (12)^b

	membranoid F (10)		membranoid G (11)		membranoid H (12)
pos	δC, typec	δHd (J in Hz)	δC, typec	δHd (J in Hz)	δC, typec	δHd (J in Hz)
1α	41.2, CH2	1.50, ov m	39.8, CH2	1.52, m	41.9, CH2	1.45, ov m
β		2.32, d (13.7)		2.23, m		2.33, d (14.3)
2α	19.9, CH2	1.69, ov m	19.9, CH2	1.73, m	20.8, CH2	1.67, m
β		1.80, m		1.80, m		1.79, m
3α	39.7, CH2	1.33, ov m	39.8, CH2	1.33, m	40.5, CH2	1.31, m
4	31.8, C		31.8, C		32.4, C
5α	50.6, CH2	1.55, d (14.2)	50.5, CH2	1.59, m	50.9, CH2	1.52, m
β		2.13, d (14.2)		2.06, m		2.16, d (14.2)
6	177.6, C		174.3, C		175.6, C
7	40.8, CH	4.73, q (6.7)	39.5, CH	4.56, q (7.3)	41.7, CH	4.64, q (7.2)
8	137.5, C		138.2, C		137.9, C
9	154.9, C		154.4, C		150.1, C
10	40.3, C		40.5, C		40.4, C
11	130.3, CH	7.76, d (8.3)	128.4, CH	7.76, d (8.3)	122.4, CH	7.65, d (8.3)
12	123.9, CH	7.73, d (8.3)	134.1, CH	7.73, d (8.3)	130.2, CH	7.30, d (8.3)
13	126.0, C		130.5, C		137.5, C
14	145.1, C		134.0, C		140.8, C
15	103.6, CH	6.14, s	92.9, CH	7.26, s	107.4, CH	5.86, s
16	168.6, C		192.5, CH	10.1, s	97.7, CH	6.98, s
17	17.7, CH3	1.73, d (7.3)	24.2, CH3	1.87, d (7.1)	17.6, CH3	1.63, d (7.1)
18	27.3, CH3	0.48, s	28.2, CH3	0.58, s	27.5, CH3	0.47, s
19	32.7, CH3	0.95, s	32.2, CH3	0.97, s	33.2, CH3	0.93, s
20	32.7, CH3	1.42, s	32.4, CH3	1.32, s	33.3, CH3	1.38, s
21	56.5, CH3	3.59, s			55.3, CH3	3.39, s
22					171.2, C
23					21.5, CH3	2.06, s
OH				5.00, bs

^aCDCl₃.

^bCD₃CN.

^c125 MHz.

^d500 MHz; ov = overlapped.