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Reaction conditions: 1 (0.5 mmol), Fe(dpm)3 (5 mol%), PhSiH3 (1.0 mmol), i-PrOH/DCE (2.0 mL + 1.0 mL), 35 °C, 2 h. Isolated yield.
Run on a gram-scale with 1 mol% Fe(dpm)3 and 1.5 equiv. PhSiH3.
Reaction for 12 h.
