Official websites use .gov
A
.gov website belongs to an official
government organization in the United States.
Secure .gov websites use HTTPS
A lock (
) or https:// means you've safely
connected to the .gov website. Share sensitive
information only on official, secure websites.
|
|---|
|
Conditions C: i. 2a (0.5 mmol), [Ir(COD)OMe]2 (0.05 mol%), Et2SiH2 (1.2 equiv.), THF, 30 °C; ii. [Ir(COD)Cl]2 (2.5 mol%), Me4Phen (6 mol%), A (1.0 equiv.), THF, 100 °C; iii. PhLi, THF, −78 °C; see the ESI for more details.
iii. KHCO3 (2.5 equiv.), H2O2 (10 equiv.), THF/MeOH (1 : 1), 50 °C.
