Table 10.
Lot-to-lot consistencya
| Reagent blank, A420nma |
Sensitivity, mA420nm·L/mgb |
Accuracy ratioc |
|||||||
|---|---|---|---|---|---|---|---|---|---|
| Lotd | Measured | Tolerance | Measured | Tol. min. | Tol. max. | Control 1 | Control 2 | Tol. min. | Tol. max. |
| 00001 | 0.056 | <0.300 | 44.7 | 40.5 | 49.5 | 1.01 | 1.05 | 0.90 | 1.10 |
| 00004 | 0.055 | <0.300 | 42.4 | 40.5 | 49.5 | 1.08 | 1.01 | 0.90 | 1.10 |
| 00014 | 0.065 | <0.300 | 45.1 | 40.5 | 49.5 | 1.07 | 0.90 | 0.90 | 1.10 |
| 00026 | 0.065 | <0.300 | 44.7 | 40.5 | 49.5 | 1.06 | 1.00 | 0.90 | 1.10 |
| 00029 | 0.068 | <0.300 | 44.9 | 40.5 | 49.5 | 1.09 | 1.01 | 0.90 | 1.10 |
| 00031 | 0.073 | <0300 | 46.2 | 40.5 | 49.5 | 1.04 | 1.00 | 0.90 | 1.10 |
| 00035 | 0.076 | <0.300 | 45.6 | 40.5 | 49.5 | 1.05 | 0.99 | 0.90 | 1.10 |
| 00037 | 0.063 | <0.300 | 44.9 | 40.5 | 49.5 | 1.07 | 1.01 | 0.90 | 1.10 |
| 00038 | 0.063 | <0.300 | 46.4 | 40.5 | 49.5 | 1.04 | 0.98 | 0.90 | 1.10 |
| 00041 | 0.065 | <0.300 | 45.2 | 40.5 | 49.5 | 1.07 | 1.03 | 0.90 | 1.10 |
| 00043 | 0.065 | <0.300 | 43.7 | 40.5 | 49.5 | 1.09 | 1.05 | 0.90 | 1.10 |
| 00044 | 0.102 | <0.300 | 43.2 | 40.5 | 49.5 | 1.09 | 1.04 | 0.90 | 1.10 |
| 00047 | 0.053 | <0.300 | 44.9 | 40.5 | 49.5 | 1.02 | 0.99 | 0.90 | 1.10 |
| Mean | 0.067 | 44.8 | 1.06 | 1.00 | |||||
| Sr | 0.012 | 1.110 | 0.027 | 0.038 | |||||
| RSDr, % | 18.6 | 2.48 | 2.50 | 3.82 | |||||
Absorbance of the reagent blank at 420 nm.
Ratio of the absorbance (in miliabsorbance) obtained with the calibrator 3 and the concentration of the same calibrator (10 mg/L).
Ratio of the concentration (mg/L) obtained in the control of the reagent and the assigned concentration of the reference material (Control 1, 8 mg/L / Control 2, 13 mg/L).
Results of several lots produced.