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. 2020 Oct 14;104(3):693–711. doi: 10.1093/jaoacint/qsaa139

Table 10.

Lot-to-lot consistencya

Reagent blank, A420nma
Sensitivity, mA420nm·L/mgb
Accuracy ratioc
Lotd Measured Tolerance Measured Tol. min. Tol. max. Control 1 Control 2 Tol. min. Tol. max.
00001 0.056 <0.300 44.7 40.5 49.5 1.01 1.05 0.90 1.10
00004 0.055 <0.300 42.4 40.5 49.5 1.08 1.01 0.90 1.10
00014 0.065 <0.300 45.1 40.5 49.5 1.07 0.90 0.90 1.10
00026 0.065 <0.300 44.7 40.5 49.5 1.06 1.00 0.90 1.10
00029 0.068 <0.300 44.9 40.5 49.5 1.09 1.01 0.90 1.10
00031 0.073 <0300 46.2 40.5 49.5 1.04 1.00 0.90 1.10
00035 0.076 <0.300 45.6 40.5 49.5 1.05 0.99 0.90 1.10
00037 0.063 <0.300 44.9 40.5 49.5 1.07 1.01 0.90 1.10
00038 0.063 <0.300 46.4 40.5 49.5 1.04 0.98 0.90 1.10
00041 0.065 <0.300 45.2 40.5 49.5 1.07 1.03 0.90 1.10
00043 0.065 <0.300 43.7 40.5 49.5 1.09 1.05 0.90 1.10
00044 0.102 <0.300 43.2 40.5 49.5 1.09 1.04 0.90 1.10
00047 0.053 <0.300 44.9 40.5 49.5 1.02 0.99 0.90 1.10
Mean 0.067 44.8 1.06 1.00
Sr 0.012 1.110 0.027 0.038
RSDr, % 18.6 2.48 2.50 3.82
a

Absorbance of the reagent blank at 420 nm.

b

Ratio of the absorbance (in miliabsorbance) obtained with the calibrator 3 and the concentration of the same calibrator (10 mg/L).

c

Ratio of the concentration (mg/L) obtained in the control of the reagent and the assigned concentration of the reference material (Control 1, 8 mg/L / Control 2, 13 mg/L).

d

Results of several lots produced.