Figure 4.
(A) Proposed Bi-H/D intermediates (9/9-D) and C-H/D reductive elimination. (B) 1H NMR spectra of 9/9-D at −40 °C; top: LiAlH4 reduction of 8b; middle: catalytic HDF of 1b; bottom: catalytic HDF of 1b using Et2SiD2.
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