| Crystal data |
| Chemical formula |
[Ru(CN)(C5H5)2(C6H12N3P)4]2[ReBr4(NO)(CH4O)0.5(C2H6O)0.5]2
|
|
M
r
|
3123.73 |
| Crystal system, space group |
Monoclinic, P21/c
|
| Temperature (K) |
296 |
|
a, b, c (Å) |
12.6027 (4), 17.7075 (6), 23.0252 (9) |
| β (°) |
101.914 (1) |
|
V (Å3) |
5027.7 (3) |
|
Z
|
2 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
6.35 |
| Crystal size (mm) |
0.48 × 0.10 × 0.03 |
| |
| Data collection |
| Diffractometer |
Bruker D8 venture diffractometer |
| Absorption correction |
Multi-scan (SADABS; Krause et al., 2015 ▸) |
|
Tmin, Tmax
|
0.485, 0.751 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
56882, 8565, 6494 |
|
R
int
|
0.079 |
| (sin θ/λ)max (Å−1) |
0.589 |
| |
| Refinement |
|
R[F2 > 2σ(F
2)], wR(F
2), S
|
0.044, 0.118, 0.99 |
| No. of reflections |
8565 |
| No. of parameters |
572 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
1.45, −1.34 |
